A kind of epitaxial wafer of light-emitting diode and its preparation method
A technology of light-emitting diodes and epitaxial wafers, which can be applied to semiconductor devices, electrical components, circuits, etc., and can solve the problems of low luminous efficiency of light-emitting diodes
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Embodiment 1
[0030] An embodiment of the present invention provides an epitaxial wafer of a light emitting diode, see figure 1 , the epitaxial wafer includes a substrate 1 and a buffer layer 2, a composite layer 3, an N-type gallium nitride layer 4, a multi-quantum well layer 5, an electron blocking layer 6 and a P-type gallium nitride layer stacked on the substrate 1 in sequence 7.
[0031] In this example, see figure 2 The composite layer 3 includes a plurality of gallium nitride layers 31 and a plurality of zinc oxide layers 32, and the plurality of gallium nitride layers 31 and the plurality of zinc oxide layers 32 are alternately stacked.
[0032] In the embodiment of the present invention, a composite layer is provided between the buffer layer and the N-type gallium nitride layer, the composite layer includes multiple gallium nitride layers and multiple zinc oxide layers alternately stacked, and the zinc oxide layer and the gallium nitride layer There is only a 1.9% lattice mismat...
Embodiment 2
[0048] The embodiment of the present invention provides a method for preparing an epitaxial wafer of a light-emitting diode, which is suitable for preparing the epitaxial wafer provided in Example 1, see image 3 , the preparation method comprises:
[0049] Step 201: growing a buffer layer on a substrate.
[0050] Specifically, this step 201 may include:
[0051] The temperature is controlled at 400° C. to 600° C., the pressure is 400 Torr to 600 Torr, and a gallium nitride layer with a thickness of 15 nm to 35 nm is grown on the sapphire substrate to form a buffer layer.
[0052] Optionally, before step 201, the preparation method may also include:
[0053]Control the temperature to 1100° C., anneal the substrate in a hydrogen atmosphere for 8 minutes, and perform nitriding treatment to clean the substrate.
[0054] Specifically, the substrate can be sapphire with [0001] crystal orientation.
[0055] Optionally, after step 201, the preparation method may further include: ...
Embodiment 3
[0079] The embodiment of the present invention provides a method for preparing an epitaxial wafer of a light-emitting diode, and the preparation method provided in this embodiment is a specific realization of the preparation method provided in Embodiment 2. see Figure 4 , the preparation method comprises:
[0080] Step 301: Control the temperature to 1100° C., anneal the substrate in a hydrogen atmosphere for 8 minutes, and perform nitriding treatment.
[0081] Step 302 : controlling the temperature to 500° C. and the pressure to 500 Torr, growing a gallium nitride layer with a thickness of 25 nm on the sapphire substrate to form a buffer layer.
[0082] Step 303: Control the temperature to 1100° C., the pressure to 500 Torr, and the duration to 7.5 minutes, and perform in-situ annealing treatment on the buffer layer.
[0083] Step 304: controlling the temperature to 1050° C. and the pressure to 300 torr, alternately growing multiple gallium nitride layers and multiple zinc...
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Abstract
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