Modified fiber for wallpaper, and production method thereof

A technology for modifying fibers and wallpapers, which is applied in fiber treatment, textiles and papermaking, and addition of inorganic compounds, etc. It can solve the problems of low tensile load of wallpapers and failure to achieve usability

Inactive Publication Date: 2018-04-13
ANHUI YINTU DECORATION MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In view of the above-mentioned prior art, the purpose of the present invention is to overcome the problem of using waste paper pulp to make wallpaper in the prior art. Although the environmental protection performance is achieved, the wal

Method used

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Examples

Experimental program
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Effect test

preparation example Construction

[0015] The present invention provides a kind of preparation method of modified fiber for wallpaper, wherein, described preparation method comprises:

[0016] 1) In the presence of a solvent, mix the sodium silicate and the dispersant, and heat in a water bath at a temperature of 35-45°C to obtain a mixture M1;

[0017] 2) Under the condition of heating in a water bath at a temperature of 35-45° C., after adding an aqueous solution of ammonium chloride dropwise to the mixture M1 prepared in step 1), discard the supernatant and take the precipitate;

[0018] 3) roasting the above-mentioned precipitate after drying to obtain granules;

[0019] 4) After adding the granules and coupling agent prepared in step 3) to the water slurry containing fibers, stirring and mixing at a temperature of 60-80° C. for 1-3 hours to obtain modified fibers for wallpaper.

[0020] In the present invention, after mixing the sodium silicate and the dispersant, the ammonium chloride aqueous solution is...

Embodiment 1

[0031] 1) In the presence of 80 parts by weight of an aqueous solution of ethanol (concentration of 15% by weight), mix 100 parts by weight of sodium silicate and 1 part by weight of polyvinylpyrrolidone, and place the mixture at a temperature of 35°C Heated in a water bath to obtain a mixture M1;

[0032] 2) Under the condition of heating in a water bath at a temperature of 35°C, add 20 parts by weight of ammonium chloride dropwise at a rate of 50 drops / min in 100 parts by weight of the mixture M1 prepared in step 1) (by a concentration of 35 parts by weight % ammonium chloride aqueous solution), discard the supernatant and get the precipitate;

[0033] 3) After drying the above precipitate at 80°C for 3h, then roasting at 400°C for 0.5h to obtain granules;

[0034] 4) After adding 40 parts by weight of granules and 5 parts by weight of KH550 silane coupling agent prepared in step 3) to 100 parts by weight of fiber-containing water slurry (waste paper: water = 45:55), place ...

Embodiment 2

[0036] 1) In the presence of 120 parts by weight of an aqueous solution of ethanol (concentration of 15% by weight), mix 100 parts by weight of sodium silicate and 5 parts by weight of polyvinylpyrrolidone, and place the mixture at a temperature of 45°C Heated in a water bath to obtain a mixture M1;

[0037] 2) Under the condition of heating in a water bath at a temperature of 45°C, add 50 parts by weight of ammonium chloride dropwise at a rate of 150 drops / min in 100 parts by weight of the mixture M1 prepared in step 1) (by a concentration of 35 parts by weight). % ammonium chloride aqueous solution), discard the supernatant and get the precipitate;

[0038] 3) After drying the above precipitate at 100°C for 5h, then roasting at 500°C for 2h to obtain granules;

[0039] 4) After adding 80 parts by weight of granules and 30 parts by weight of KH550 silane coupling agent prepared in step 3) to 100 parts by weight of fiber-containing water slurry (waste paper: water = 45:55), p...

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PUM

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Abstract

The invention discloses a modified fiber for wallpaper, and a production method thereof. The production method comprises the following steps: 1, mixing sodium silicate with a dispersant in the presence of a solvent, and carrying out water bath heating at 35-45 DEG C to prepare a mixture M1; 2, dropwise adding an aqueous solution of ammonium chloride to the mixture M1 prepared in step 1 under a 35-45 DEG C water bath heating condition, abandoning the obtained supernatant, and taking the obtained precipitate; 3, drying the precipitate, and calcining the dried precipitate to prepare granules; and4, adding the granules prepared in step 3 and a coupling agent to a water slurry containing fibers, and stirring and mixing all above materials at 60-80 DEG C for 1-3 h to produce the modified fiberfor wallpaper. The modified fiber produced through the above materials and the method can effectively improve the tension load of wallpaper made of waste paper pulp.

Description

technical field [0001] The invention relates to the field of fiber materials for wallpaper, in particular to modified fibers for wallpaper and a preparation method thereof. Background technique [0002] Wallpaper is widely used for its rich pattern and good performance, as well as the safety of materials, so its usage is also increasing. And adopt waste paper pulp to make wallpaper, although reached environmental protection performance, often the wallpaper tensile load of making is lower, makes it can not reach better usability. [0003] Therefore, it is an urgent problem to be solved in the present invention to provide a modified fiber for wallpaper and a preparation method thereof that still have a good tensile load under the premise of utilizing waste paper pulp. Contents of the invention [0004] In view of the above-mentioned prior art, the purpose of the present invention is to overcome the problem of using waste paper pulp to make wallpaper in the prior art. Althou...

Claims

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Application Information

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IPC IPC(8): D06M11/79D21H17/69D21H17/68
CPCD06M11/79D21H17/68D21H17/69
Inventor 凌清明周玉斌吴中建莫秀斌
Owner ANHUI YINTU DECORATION MATERIALS CO LTD
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