A kind of preparation method of organic gas adsorption purification agent
A technology for adsorbing purifiers and organic gases, applied in catalyst activation/preparation, chemical instruments and methods, inorganic chemistry, etc., can solve problems such as low adsorption performance and poor interfacial adhesion between materials, and achieve large specific surface area and fast carbonization Speed, strong catalytic effect
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[0021] A preparation method of an organic gas adsorption purification agent, comprising the following steps:
[0022] (1) Mix ethyl orthosilicate, absolute ethanol, N,N-dimethylformamide and water in a mass ratio of 2:3:1:10 for later use;
[0023] (2) Put the spinning solution in the electrospinning apparatus, wrap the receiver with aluminum foil, and collect the as-spun fibers on the aluminum foil. The process parameters of the spinning process are positive pressure 15kV, negative pressure 1.5kV, and advance rate 0.04 mm / min, the receiving rate is 30r / min, the distance between the needle and the receiver is 15cm, and the ambient temperature is 30°C. After the spinning is completed, let it stand at room temperature for one day to obtain the as-spun fiber, and then place it in an oven to raise the temperature. Solidify at 160°C for 60 minutes, take it out and put it into a tube furnace, raise the temperature from room temperature to 750°C at a rate of 5°C / min under a nitrogen ...
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