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Preparation method of water-retaining agent for agricultural facilities

A water-retaining agent and facility technology, which is applied in agriculture, chemical instruments and methods, agricultural machinery and implements, etc., can solve the problems of environmental pollution stability, difficult decomposition of water-retaining agent, etc., to prevent water evaporation loss, high stability, and saving. cost effect

Inactive Publication Date: 2018-05-04
ZHEJIANG OCEAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to overcome the problems of the prior art that the water-retaining agent is not easy to decompose, pollute the environment and have poor stability, and provide a method for preparing a water-retaining agent that can be naturally decomposed and has good stability

Method used

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  • Preparation method of water-retaining agent for agricultural facilities
  • Preparation method of water-retaining agent for agricultural facilities

Examples

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Embodiment 1

[0025] A preparation method for water-retaining agent for agricultural facilities, comprising the following steps:

[0026] 1) Pulverize mussel shells, pass through a 50-mesh sieve, and then add phosphoric acid with a content of 83% to the sieved powder, wherein the mass ratio of mussel shell sieved powder to phosphoric acid is 1:0.2g / mL, React for 1 hour with assistance, control the ambient temperature at 15°C, and continue stirring for 2 hours to obtain raw material 1;

[0027] 2) Dissolve the crayfish shells with 2mol / L hydrochloric acid, filter and add 40% sodium hydroxide solution to the filter residue, wherein the mass ratio of crayfish shells to sodium hydroxide is 1:2, boil 2h, cooled to room temperature to obtain raw material 2;

[0028] 3) Mix raw materials 1 and 2 according to the ratio of 1:0.02, and stir continuously at 5° C. for 1 hour to obtain the final moisturizer.

[0029] Among them, the raw materials in raw material 2 have been pretreated, and the pretrea...

Embodiment 2

[0035] A preparation method for water-retaining agent for agricultural facilities, comprising the following steps:

[0036] 1) Pulverize the mussel shells, pass through a 60-mesh sieve, and then add phosphoric acid with a content of 85% to the sieved powder, wherein the mass of the mussel shells sifted powder and the volume ratio of phosphoric acid are 1:2g / mL. React at low temperature for 5 hours, control the ambient temperature at 20°C, and continuously stir for 10 hours to obtain raw material 1;

[0037] 2) Dissolve the crayfish shells with 2.2mol / L hydrochloric acid, filter and add 45% sodium hydroxide solution to the filter residue, wherein the volume ratio of the mass of crayfish shells to sodium hydroxide is 1:4, Boiling for 4h, cooling to room temperature to obtain raw material 2;

[0038] 3) Mix raw materials 1 and 2 according to the ratio of 1:0.05, and stir continuously at 10° C. for 3 hours to obtain the final moisturizer.

[0039] Among them, the raw materials i...

Embodiment 3

[0045] A preparation method for water-retaining agent for agricultural facilities, comprising the following steps:

[0046] 1) Pulverize mussel shells, pass through a 70-mesh sieve, and then add phosphoric acid with a content of 88% to the sieved powder, wherein the mass of mussel shells sifted powder and the volume ratio of phosphoric acid are 1:5g / mL. React at low temperature for 10 hours, control the ambient temperature at 25°C, and continuously stir for 12 hours to obtain raw material 1;

[0047]2) Dissolve the crayfish shells with 2.5mol / L hydrochloric acid, filter and add 50% sodium hydroxide solution to the filter residue, wherein the volume ratio of the mass of crayfish shells to sodium hydroxide is 1:5, Boil for 6 hours, cool to room temperature to obtain raw material 2;

[0048] 3) Mix the raw materials 1 and 2 according to the ratio of 1:0.1, and stir continuously at 15°C for 5 hours to obtain the final moisturizer.

[0049] Among them, the raw materials in raw ma...

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Abstract

The invention relates to the technical field of a water-retaining agent, and discloses a preparation method of a water-retaining agent for agricultural facilities. The preparation method of the water-retaining agent comprises the following steps of (1) crushing mussel shells and then adding phosphoric acid into screened powder; performing reaction under the assistance of ultrasonic waves; performing continuous stirring to obtain a raw material 1; (2) dissolving cray shell by hydrochloric acid; after filtering, adding a sodium hydroxide solution into filter slag; performing boiling and coolingto room temperature to obtain a raw material 2; (3) mixing the raw materials 1 and 2 according to a certain ratio; performing continuous stirring to obtain a final product of the water-retaining agent. The water-retaining agent provided by the invention has the advantages that the green and environment-friendly effects are achieved; the water-retaining performance is stable.

Description

technical field [0001] The invention relates to the technical field of water-retaining agents, in particular to a preparation method for water-retaining agents for agricultural facilities. Background technique [0002] Moisture is one of the most important factors in agricultural production, and the whole process of crop growth and development requires water. Water shortages such as droughts can have a severe impact on agricultural production, leading to eventual crop failures. Therefore, moisturizing and water retention are of great significance to agricultural production. At present, it is reported in the literature that water retaining agents are mainly synthetic resins. Synthetic resin water retaining agents have high production efficiency, low cost, good water absorption, and high gel strength; however, they have poor salt resistance, are not easy to degrade, and pollute the environment. This kind of water-retaining agent is suitable for relatively arid areas, and its...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K17/40C09K101/00
CPCC09K17/40C09K2101/00
Inventor 刘俊稚葛亚明孙静亚夏松养
Owner ZHEJIANG OCEAN UNIV