A kind of biodegradable environmental protection lubricating oil
A technology of biodegradation and lubricating oil, applied in the field of lubricating oil, can solve the problems of poor oxidation stability of vegetable oil, poor low temperature performance and small application field, and achieve the effects of good biodegradability, good low temperature performance and low price
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Embodiment 1
[0025] A kind of biodegradable environment-friendly lubricating oil, comprises the raw material of following weight part:
[0026]
[0027] Wherein, the preparation method of the 2,5-furandicarboxylic acid starch ester comprises the following steps: dissolving 20 g of 2,5-furandicarboxylic acid in 180 g of tetrahydrofuran, and then adding 10 g of starch, 30 g of carbodiimide, 4-diimide Methylaminopyridine 15g, stirred in an ice-water bath for 2 hours, then refluxed and stirred at 40°C for 18 hours, then filtered, diluted with tetrahydrofuran, washed 3 times with water, washed 4 times with saturated saline, absorbed by anhydrous magnesium sulfate, filtered , and then remove the solvent by rotary evaporation at 50°C;
Embodiment 2
[0029] A kind of biodegradable environment-friendly lubricating oil, comprises the raw material of following weight part:
[0030]
[0031] Wherein, the preparation method of the 2,5-furandicarboxylic acid starch ester comprises the following steps: dissolving 20 g of 2,5-furandicarboxylic acid in 200 g of tetrahydrofuran, and then adding 11 g of starch, 30 g of carbodiimide, 4-diimide Methylaminopyridine 20g, stirred in an ice-water bath for 2.3 hours, then refluxed and stirred at 43°C for 20 hours, then filtered, diluted with dichloromethane, washed 4 times with water, washed 5 times with saturated saline, and absorbed by anhydrous magnesium sulfate , filtered, and then rotary evaporated at 53 ° C to remove the solvent;
Embodiment 3
[0033] A kind of biodegradable environment-friendly lubricating oil, comprises the raw material of following weight part:
[0034]
[0035] Wherein, the preparation method of starch 2,5-furandicarboxylate comprises the following steps: dissolving 20 g of 2,5-furandicarboxylic acid in 220 g of tetrahydrofuran, and then adding 12 g of starch, 36 g of carbodiimide, 4-diimide Methylaminopyridine 22g, stirred in an ice-water bath for 2.5 hours, then refluxed and stirred at 45°C for 22 hours, then filtered, diluted with ethyl acetate, washed 5 times with water, washed 6 times with saturated saline, and absorbed by anhydrous magnesium sulfate , filtered, and then rotary evaporated at 56 ° C to remove the solvent;
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