Hydroxyapatite powder with upconversion fluorescence and superparamagnetism and preparation method thereof
A technology of hydroxyapatite and superparamagnetism, which is applied in the fields of biomedical materials and biomedical engineering, can solve the problems of non-fluorescence characteristics, inability to realize material distribution and bone formation process, bone tissue regeneration and reconstruction, and achieve fluorescence High intensity, avoid tissue autofluorescence interference, and promote bone formation
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Embodiment 1
[0035] The steps for preparing HA:Yb+Ho / 0.25Fe powder in this example are as follows:
[0036] (1) In a 50mL hydrothermal reaction kettle, add 0.5g octadecylamine and 4mL oleic acid into 16mL ethanol, mix well to obtain an alcohol solution containing octadecylamine and oleic acid, then add 9mL calcium nitrate aqueous solution (Ca 2+ molar concentration is 0.2mol / L) to obtain the first mixed solution, in the first mixed solution, add 2mL Yb (NO 3 ) 3 Aqueous solution [contains Yb(NO 3 ) 3 0.36mmol] and 2mL Ho(NO 3 ) 3 Aqueous solution [contains Ho(NO 3 ) 3 0.036mmol] to obtain the mixed solution, at 70°C, under stirring conditions, 9mL sodium phosphate aqueous solution (PO 4 3- The molar concentration is 0.12mol / L) is added dropwise in the second mixed solution of gained, during the dropping process, by adding ammonia water, the pH value of the reaction system is maintained at 10, and then the resulting suspension is packed into the hydrothermal reaction kettle after ...
Embodiment 2
[0039] The steps of preparing HA:Yb+Ho / 0.5Fe powder in this embodiment are as follows:
[0040] (1) In a 50mL hydrothermal reaction kettle, add 0.5g octadecylamine and 4mL oleic acid into 16mL ethanol, mix well to obtain an alcohol solution containing octadecylamine and oleic acid, then add 9mL calcium nitrate aqueous solution (Ca 2+ molar concentration is 0.2mol / L) to obtain the first mixed solution, in the first mixed solution, add 2mL Yb (NO 3 ) 3 Aqueous solution [contains Yb(NO 3 ) 3 0.36mmol] and 2mL Ho(NO 3 ) 3 Aqueous solution [contains Ho(NO 3 ) 3 0.036mmol] to obtain the mixed solution, at 50 °C under stirring conditions, 9mL sodium phosphate aqueous solution (PO 4 3- The molar concentration is 0.12mol / L) is added dropwise in the second mixed solution of the gained, during the dropping process, the pH value of the reaction system is maintained at 9 by adding ammonia water, and then the resulting suspension is packed into the hydrothermal reaction kettle aft...
Embodiment 3
[0043] The steps of preparing HA:Yb+Ho / 1Fe powder in this embodiment are as follows:
[0044] (1) In a 50mL hydrothermal reaction kettle, add 0.5g octadecylamine and 4mL oleic acid into 16mL ethanol, mix well to obtain an alcohol solution containing octadecylamine and oleic acid, then add 9mL calcium nitrate aqueous solution (Ca 2+ molar concentration is 0.2mol / L) to obtain the first mixed solution, in the first mixed solution, add 2mL Yb (NO 3 ) 3 Aqueous solution [contains Yb(NO 3 ) 3 0.36mmol] and 2mL Ho(NO 3 ) 3 Aqueous solution [contains Ho(NO 3 ) 3 0.036mmol] to obtain the mixed solution, at 50 °C under stirring conditions, 9mL sodium phosphate aqueous solution (PO 4 3- The molar concentration is 0.12mol / L) is added dropwise in the second mixed solution of gained, during the dropping process, by adding ammonia water, the pH value of the reaction system is maintained at 10, and then the resulting suspension is packed into the hydrothermal reaction kettle after t...
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