A kind of preparation method and application of hemp essential oil
A technology of hemp essence and hemp oil, which is applied in essential oils/fragrances, skin care preparations, pharmaceutical formulations, etc., and can solve the problems of hemp oil with many impurities, low oil yield, and poor stability
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[0034] A preparation method of hemp essential oil, the process route is as follows figure 1 Shown, described method is prepared by following process:
[0035] (1) Hemp seed is dried at low temperature (controlling moisture content 5%-20%), pulverized, and sieved (10-60 mesh);
[0036] (2) Put the sieved powder into the extraction kettle, check the air tightness of the instrument; turn on the supercritical cooling device, and when the temperature drops below 5 degrees, set the extraction carbon dioxide temperature (30-50°C), and open the When the heating switch reaches the set temperature value, gradually adjust the extraction pressure to the specified value (25-45MPa). When the pressure rises to the specified value, open the valve of the collection bottle and adjust the extraction CO 2 Flow rate (4-8L / min), and start to record the extraction time (1-4h), until the extraction is completed;
[0037] (3) The hemp oil after supercritical is decolorized with activated clay (decol...
Embodiment 1
[0041] A preparation method of hemp essential oil, comprising the steps of:
[0042] (1) Hemp seed pretreatment: place the hemp seed in an environment of 60° C. and dry until the water content is 10%, pulverize, pass through a 20-mesh sieve, and obtain hemp seed powder;
[0043] (2) Extraction: put the hemp seed powder into the extraction kettle, turn on the supercritical cooling device, and when the temperature drops below 5°C, set the extraction CO 2 The temperature is 39.32°C, and the heating switch is turned on. When the set temperature value (39.32°C) is reached, the extraction pressure is gradually adjusted to 36.6MPa. When the pressure rises to the specified value (36.6MPa), the valve of the collection bottle is opened to adjust the extraction CO 2 The flow rate was 7.02L / min, and the extraction time was recorded, and the extraction was finished after 3.5h to obtain hemp oil;
[0044] (3) decolouring: the hemp oil after extraction is decolorized with active clay, the d...
Embodiment 2
[0048] A preparation method of hemp essential oil, comprising the steps of:
[0049] (1) hemp seed pretreatment: place the hemp seed in an environment of 55° C. and dry until the water content is 15%, pulverize, pass through a 30-mesh sieve, and obtain hemp seed powder;
[0050] (2) Extraction: put the hemp seed powder into the extraction kettle, turn on the supercritical cooling device, and when the temperature drops below 5°C, set the extraction CO 2 The temperature is 32°C, and the heating switch is turned on. When the set temperature is reached, the extraction pressure is gradually adjusted to 40MPa. When the pressure rises to the specified value, the valve of the collection bottle is opened, and the extraction CO is adjusted. 2 The flow rate is 6L / min, and the extraction time is recorded, and the extraction ends after 2 hours to obtain hemp oil;
[0051] (3) decolorization: the hemp oil after extraction is decolorized with activated clay, the decolorization time is 20min...
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