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Production device for 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene

A technology for tert-butylbenzene and production equipment, which is applied in the preparation of nitro compounds, hydrocarbons, hydrocarbons, etc., can solve the problems of very good use effect, complexity, and increased epidermal absorption of drugs.

Inactive Publication Date: 2018-07-03
成都盛金缘餐饮文化传播有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] 2,4,6-Trinitro-3,3-dimethyl-5-tert-butylbenzene is used as a fixative and modifier, and is widely used in soaps, shampoos, face powders and other daily flavors. It is very effective to be used in flavors such as pine and pine
Musk xylene is also used as a transdermal agent for many traditional Chinese medicine plasters to increase the epidermal absorption of drugs, and has sedative and analgesic effects. Most of the existing production equipment is more complicated. 2,4,6-Trinitro -3,3-Dimethyl-5-tert-butylbenzene is used as an analgesic, and the quality of its production equipment is of great economic significance for improving product quality and reducing the content of by-products

Method used

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  • Production device for 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene
  • Production device for 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene
  • Production device for 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene

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example 1

[0008] Production raw materials and dosage

[0009] tert-butanol

industrial grade

80

concentrated nitric acid

Industrial grade, 60%

200

hydrochloric acid

industrial grade

120

concentrated sulfuric acid

Industrial grade, 90%

400

m-xylene

industrial grade

150

[0010] The production equipment of 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene mainly includes: chlorination tank (D101), condensation tank (D102), neutralization washing tank (D103 ), delivery pump (P101~P105), nitrification tank (D104), washing tank (D105), crystallization tank (D106), among which, delivery pump (P101) is connected with chlorination tank (D101) and condensation tank (D102) respectively Connection, the delivery pump (P104) is connected with the nitrification tank (D104) and the water washing tank (D105) respectively, among which, the impeller diameter of the delivery pump (P103) is 107-112mm, the jacket capacity of the...

example 2

[0015] Production raw materials and dosage

[0016]

[0017]

[0018] The production equipment of 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene mainly includes: chlorination tank (D101), condensation tank (D102), neutralization washing tank (D103 ), delivery pump (P101~P105), nitrification tank (D104), washing tank (D105), crystallization tank (D106), among which, delivery pump (P101) is connected with chlorination tank (D101) and condensation tank (D102) respectively Connection, the delivery pump (P104) is connected with the nitrification tank (D104) and the water washing tank (D105) respectively, among which, the impeller diameter of the delivery pump (P103) is 112mm, the jacket capacity of the washing tank (D105) is 280L, and the crystallization tank (D106) The diameter of the pot is 650mm.

[0019] 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene production device, the production process is: add tert-butanol and excess hydrochloric acid into the chlorination tank, ...

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Abstract

The invention discloses a production device for 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene. The production device mainly includes a chlorination tank (D101), a condensation tank (D102), a neutralization water washing tank (D103), delivery pumps (P101-P105), a nitrification tank (D104), a water washing tank (D105), and a crystallization tank (D106), wherein one delivery pump (P101) is connected with the chlorination tank (D101) and the condensation tank (D102), one delivery pump (P104) is connected with the nitrification tank (D104) and the water washing tank (D105), and one delivery pump(P103) has an impeller diameter of 107-112mm.

Description

technical field [0001] The invention relates to a compound synthesis device, in particular to a production device for 2,4,6-trinitro-3,3-dimethyl-5-tert-butylbenzene. Background technique [0002] 2,4,6-Trinitro-3,3-dimethyl-5-tert-butylbenzene is used as a fixative and modifier, and is widely used in soaps, shampoos, face powders and other daily flavors. It is very effective in flavors such as pine wood and pine wood. Musk xylene is also used as a transdermal agent for many traditional Chinese medicine plasters to increase the epidermal absorption of drugs, and has sedative and analgesic effects. Most of the existing production equipment is more complicated. 2,4,6-Trinitro -3,3-dimethyl-5-tert-butylbenzene is used as an analgesic, and the quality of its production equipment is of great economic significance for improving product quality and reducing the content of by-products. Contents of the invention [0003] The object of the present invention is to provide a product...

Claims

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Application Information

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IPC IPC(8): C07C205/06C07C201/08C07C17/16C07C19/01C07C2/86C07C15/02
CPCC07C2/861C07C17/16C07C19/01C07C201/08C07C15/02C07C205/06
Inventor 彭响亮
Owner 成都盛金缘餐饮文化传播有限公司
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