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Method for reducing viscosity of flotation barite concentrate

A barite and concentrate technology, applied in flotation, solid separation, etc., can solve the problems of barite powder viscosity exceeding, increasing the shear force of barite slurry, etc.

Active Publication Date: 2018-08-28
BEIJING RESEARCH INSTITUTE OF CHEMICAL ENGINEERING AND METALLURGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the barite powder produced by direct mining and gravity separation process, there is generally no problem of excessive viscosity, but for the barite powder obtained by flotation method, the mineral has a strong hydrophobic effect due to the adsorption of flotation agents on the surface of the barite , which increases the shear force of the barite pulp, resulting in the viscosity of the barite powder exceeding the requirements of the national standard

Method used

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  • Method for reducing viscosity of flotation barite concentrate

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] In Example 1, under the same calcination time and different calcination temperatures, the calcination temperature that can make the barite powder viscosity reach the standard is investigated.

[0017] The test ore sample is barite powder prepared by flotation method, the content of -200 mesh is 95%, the content of barium sulfate is 93.22%, and the density of barite powder is 4.22g / cm 3 , The viscosity of barite powder is 170Pa·s.

[0018] The test steps and procedures are as follows:

[0019] 1) Place 50g of ore sample evenly in a porcelain crucible, the thickness of the ore layer is 1cm. After the temperature of the muffle furnace was raised to 200°C, the temperature was kept constant. Carefully put the open-covered porcelain crucible into the muffle furnace with crucible tongs for firing, and use the crucible tongs to turn the sample to fully contact with the air during the firing process. The ore samples were roasted in the muffle furnace for 15 minutes.

[0020]...

Embodiment 2

[0027] Example 2 is to investigate the shortest time for the ore powder to achieve complete drug removal and the viscosity of the barite powder to reach the standard at different calcination temperatures.

[0028] The test ore sample is barite powder prepared by flotation method, the content of -200 mesh is 95%, the content of barium sulfate is 93.22%, and the density of barite powder is 4.22g / cm 3 , The viscosity of barite powder is 170Pa·s.

[0029] The test steps and procedures are as follows:

[0030] 1) Place 25g of ore sample evenly in a porcelain crucible, and the thickness of the ore layer is 0.5cm. The calcination temperature was set to 400°C, 500°C, and 600°C in sequence.

[0031] 2) After raising the temperature of the muffle furnace to the set temperature, keep the temperature constant. Use crucible tongs to carefully put the open-covered porcelain crucible into the muffle furnace for roasting. At the same roasting temperature, gradually shorten the roasting tim...

Embodiment 3

[0038] A method for reducing the viscosity of flotation barite concentrate, comprising the following steps:

[0039] S1: Take 10g of flotation barite concentrate and put it evenly in the crucible, the concentrate particle size is -200 mesh, accounting for 50%, and the thickness of the ore layer is 0.2cm;

[0040] S2: After raising the temperature of the muffle furnace to 200°C, keep the constant temperature, and use the crucible tongs to put the open-covered porcelain crucible into the muffle furnace for roasting; the roasting time of the ore sample in the muffle furnace is 0.1min;

[0041] S3: Take out the roasted ore sample, after cooling to room temperature, test the drug removal effect with water;

[0042] S4: The barite concentrate after roasting and drug removal is made into a density of 2.50g / cm according to the operation regulations of GBT5005-2010 3 The barite powder was suspended in distilled water, and after stirring and curing for 24 hours, the apparent viscosity ...

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Abstract

The invention discloses a method for reducing viscosity of the flotation barite concentrate. According to barite powder obtained through a flotation method, due to the fact that a collecting agent isadsorbed on the surface of the barite powder, the barite powder is hydrophobic, when the viscosity measurement is carried out, the barite ore pulp is large in shearing force, the viscosity can not meet the national standard requirements, and then sales can not be carried out. In order to solve the problems that a conventional wet-process scrubbing method is incomplete in reagent removal, is unstable in viscosity index, and the like, the research invents a low-medium-temperature roasting reagent removing process which can rapidly and thoroughly remove the reagent adsorbed on the surface of thebarite, greatly reduce the viscosity of the barite powder ore pulp, and enable the viscosity index to meet the requirements of GBT5005-2010.

Description

technical field [0001] The invention belongs to the technical requirement field of drilling grade barite powder, relates to a method for reducing the viscosity of barite powder, in particular to a method for reducing the viscosity of flotation barite concentrate. Background technique [0002] Barite is a non-metallic mineral product mainly composed of barium sulfate, with a hardness of 3 to 3.5 (Mohs), and a specific gravity of 4.3 to 4.7. It has the characteristics of large specific gravity, low hardness and brittleness. Barite is a very important non-metallic mineral raw material with a wide range of industrial uses. [0003] Drilling mud weighting agent is one of the most important uses of barite. Drilling grade barite powder can be produced from single ore or mixed ore, it can be the product of direct mining, or it can be produced by washing, shaking table, jigging or floating Choose products that have been treated with synergistic methods. According to the requirement...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03D1/08
CPCB03D1/08
Inventor 刘志超李广李春凤强录德赵凤岐牛玉清唐宝彬
Owner BEIJING RESEARCH INSTITUTE OF CHEMICAL ENGINEERING AND METALLURGY