A method for improving the quality of the five-line product of a lubricating oil-type decompression partition tower

A clapboard column and lubricating oil technology, applied in the direction of lubricating oil distillation, separation methods, chemical instruments and methods, etc., can solve problems such as large reflux ratio, unfavorable separation economic benefits, and inability to be used as lubricating oil base oil

Active Publication Date: 2020-04-24
TIANJIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, since the distillation range of the sidedraw product is limited by thermodynamics and the nature of the distillation operation
Minus five-line fraction overlaps heavily with adjacent lube oil fractions and reduced bottom bituminous oils, resulting in poor quality products that cannot be used as lube base stocks
Generally speaking, obtaining high-purity side stream products requires a large reflux ratio and a large number of trays, which is not conducive to improving the economic benefits of separation

Method used

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  • A method for improving the quality of the five-line product of a lubricating oil-type decompression partition tower
  • A method for improving the quality of the five-line product of a lubricating oil-type decompression partition tower
  • A method for improving the quality of the five-line product of a lubricating oil-type decompression partition tower

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] In order to improve the quality of lubricating oil produced by the fifth-line product so that the distillation range is less than 50°C, a certain device adopts the following figure 2 The lower partition column shown is applied to the lubricating oil type vacuum column scheme. The normal bottom residue (14) to be separated is heated by the heating furnace (5) and enters from the middle of the pre-fractionation section, and the liquid phase is extracted from the bottom of the tower as a vacuum residue (22) after steam stripping (16) at the bottom of the tower, and the gas phase Go to the public rectification section, and recover the heat in the tower through the first middle section circulation (6), the second middle section circulation (7), and the third middle section circulation (8). After further separation, the product diesel oil (17) is obtained, the second-line stripping tower (9) is used to obtain the second-line lubricating oil fraction (18), and the third-line ...

Embodiment 2

[0040] In order to improve the quality of the lubricating oil of the five-line product, a device adopts the following image 3The partition tower shown is applied to the lubricating oil type vacuum tower scheme. The normal bottom residue (14) to be separated is heated by the heating furnace (5) and enters from the middle of the pre-fractionation section, and the liquid phase is extracted from the bottom of the tower as a vacuum residue (22) after steam stripping (16) at the bottom of the tower, and the gas phase Go to the public rectification section, and recover the heat in the tower through the first middle section circulation (6), the second middle section circulation (7), and the third middle section circulation (8). After further separation, the product diesel oil (17) is obtained, the second-line stripping tower (9) is used to obtain the second-line lubricating oil fraction (18), and the third-line stripping tower (10) is used to obtain the third-line lubricating oil fra...

Embodiment example 2

[0041] Table 5 Main operating conditions of the device in implementation case 2

[0042]

[0043]

[0044] Table 6 Implementation Case 2 Product Properties

[0045]

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PUM

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Abstract

The invention relates to a method for improving quality of a vacuum fifth line product of a lubricating oil type vacuum separator tower, and a novel separator tower is introduced in a conventional lubricating oil type vacuum tower. A lower right angle separator is adopted, one side of the vertical section of the separator is used for feeding, the other side of the vertical section of the separatoris used for discharging, the horizontal section of the discharge side of the separator is connected with a tower wall by welding, and the separator tower is divided into three working sections, respectively comprising a pre-fractionation section, a common rectification section and a vacuum fifth line collection section. Normal bottom residue oil to be separated is heated by a heating furnace, enters from the middle of the pre-fractionation section, and is stripped by tower bottom steam, after the stripping, a liquid phase as vacuum residue oil is discharged from the bottom of the tower, a gasphase is sent to the common rectification section, and further separated by a side stripping tower to obtain product diesel and vacuum second line, vacuum third line and vacuum fourth lubricating oil. A stream of steam is introduced in the lower part of a vacuum fifth-line collecting section for stripping, and the vacuum fifth-line lubricating oil product is collected at the bottom. Under the premise of no increasing of the energy consumption of a vacuum furnace, the distillation range of the vacuum fifth-line lubricating oil product and overlapping degree with adjacent products are significantly reduced, and the method is used in the design of a new tower, also in the technical transformation of an old tower.

Description

technical field [0001] The invention belongs to the field of petroleum refining, and relates to a method for improving the quality of the five-line product of a lubricating oil type decompression partition tower. Background technique [0002] Petroleum refining industry is one of the most important pillar industries in the national economy. Its various products are widely used and involve all aspects of national economy, national defense construction and people's life. Atmospheric and vacuum distillation is the first process in the petroleum refining industry and the leader of the entire petroleum refining industry, occupying an important position. The design of atmospheric and vacuum distillation directly determines the yield and quality of petroleum distillate products, and has a decisive impact on the economic benefits of the entire refinery. [0003] Lubricating oil is a high value-added petroleum refined product, which is refined by a fuel-lubricating oil type atmosphe...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10G7/00B01D3/14B01D3/16
CPCB01D3/166C10G7/003C10G2300/1062
Inventor 孙津生崔承天陈金财刘思瑶
Owner TIANJIN UNIV
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