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Dry slurry material preparation technology

A dry-process slurry and process technology, applied in the direction of mixing methods, electrode manufacturing, mixer accessories, etc., can solve the problems of high equipment investment cost, complicated operation process, and long batching cycle time, so as to improve production efficiency and equipment utilization rate , The effect of simplifying the batching operation process and shortening the mixing time

Inactive Publication Date: 2018-10-12
广州云通锂电池股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Disadvantages of the existing wet batching method: the batching cycle time is as long as 8-9 hours; the operation process is complicated and cumbersome, it needs to add materials 5-6 times, scrape the wall 5-6 times, and the production efficiency is low
[0006] Disadvantages of the existing dry batching method: the batching cycle time is longer at 7-8 hours; it needs to be equipped with special equipment for glue mixing, the equipment investment cost is high and the workshop area demand is high, the operation process is complicated, and it needs to add material 4 times, scrape the wall 4 times, and produce low efficiency

Method used

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Effect test

Embodiment 1

[0053] a. Dry powder mixing: Add 94.7wt% of lithium cobaltate, superconducting carbon black super-P 2.5wt%, KS6 1wt% and RF9151.8wt% into the batching mixing tank, stirring at medium speed for 30 minutes, revolutions per minute, Disperse at 500 revolutions per minute, and control the powder temperature at 15°C during the dry powder process;

[0054] b. Slurry kneading: (1) Add 28% of the total weight of lithium cobaltate with N-methylpyrrolidone and stir at low speed for 2 minutes, with 15 revolutions per minute;

[0055] (2) Stir at medium and low speed for 5 minutes, revolution at 27 revolutions per minute;

[0056] (3) Stirring at medium speed for 30 minutes, revolution at 32 revolutions per minute;

[0057] (4) Wall scraping and high-speed stirring for 50 minutes, revolution at 40 revolutions per minute, and dispersion at 500 revolutions per minute; the material temperature during the slurry kneading and stirring process should be controlled at 15°C;

[0058] c. High-viscosity stir...

Embodiment 2

[0064] This embodiment discloses a dry slurry preparation process, including the following steps:

[0065] a. Dry powder mixing: add 93wt% of nickel cobalt manganese lithium, KS63wt%, super-P 3wt% and PH10011wt% into the batching stirring tank, stirring at medium speed for 25 minutes, stirring speed of revolution 30 revolutions / min, dispersion 500 revolutions / Minutes, the temperature of the powder in the dry powder process is controlled at 30°C.

[0066] b. Slurry kneading: (1) Add 16% of the total weight of lithium nickel cobalt manganese oxide with N-methylpyrrolidone and stir at low speed for 2 minutes, with a revolution of 17 revolutions per minute;

[0067] (2) Stir at medium and low speed for 2 minutes, revolution at 25 revolutions per minute;

[0068] (3) Stirring at medium speed for 15 minutes, revolutions per minute;

[0069] (4) Wall scraping and high-speed stirring for 40 minutes, 42 revolutions per minute for revolution, and 520 revolutions per minute for dispersion; the t...

Embodiment 3

[0076] A dry slurry preparation process of this embodiment includes the following steps:

[0077] a. Dry powder mixing: Add compound graphite 97.5wt%, SFG-6 1wt% and 1.5wt% BVH8 into the batching stirring tank, stirring at medium speed for 45 minutes, stirring speed of revolution 30 revolutions / min, dispersion 500 revolutions / min, dry powder The temperature of the process powder is controlled at 18°C.

[0078] b. Slurry kneading: (1) Add a solvent containing 64% of the total weight of the composite graphite and stir at low speed for 2 minutes, and revolution at 16 revolutions per minute;

[0079] (2) Stir at medium and low speed for 2 minutes, revolution at 26 revolutions per minute;

[0080] (3) Stirring at medium speed for 20 minutes, revolution at 31 revolutions per minute;

[0081] (4) Wall scraping and high-speed stirring for 45 minutes, revolution of 41 revolutions per minute, and dispersion of 510 revolutions per minute; the material temperature during the slurry kneading and st...

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Abstract

The invention discloses a dry slurry material preparation technology. The dry slurry material preparation technology comprises the following steps: a, mixing dry powders, namely adding active materials, a conducting agent and an adhesive-bonding agent into a material agitator, and carrying out medium-speed agitating for 25-45 minutes, wherein the temperature of the powder materials is controlled at 15-30 DEG C during the whole dry-agitating process; b, kneading slurry materials, namely (1) adding a solvent and carrying out agitating at a low speed for 2-5 minutes, (2) carrying out agitating ata medium-low speed for 2-5 minutes, (3) carrying out agitating at a medium speed for 15-30 minutes and (4) carrying out wall-scraping agitating at high speed for 40-50 minutes, wherein the material temperature is controlled at 15-30 DEG C during the whole kneading and agitating process of the slurry material; c, carrying out high-viscosity agitating, namely scraping the wall, adding a solvent, and carrying out high-speed agitating for 40-45 minutes, wherein the temperature of the slurry material is controlled within the range of 25-35 DEG C; d, carrying out low-viscosity agitating, namely scraping the wall, adding a solvent, and carrying out medium-speed agitating for 60-70 minutes, wherein the temperature of the slurry material is controlled within the range of 30-45 DEG C; and e, adjusting viscosity, namely adding a solvent, and carrying out medium-speed agitating for 30-32 minutes, wherein the temperature of the slurry material is controlled within the range of 30-45 DEG C. Compared with existing technologies, the dry slurry material preparation technology is capable of shortening the time of the material-blending cycle by 40-50%; and thus, material-blending operations are simplified so as to improve production efficiency and equipment utilization rate.

Description

Technical field [0001] The invention relates to the technical field of slurry preparation, in particular to a dry slurry preparation process. Background technique [0002] At present, the methods commonly used for slurry preparation in the lithium-ion battery production process are divided into two types: wet batching process and dry batching process, of which wet method and dry method each account for about half. Currently, double planetary vacuum mixers are commonly used in lithium-ion battery ingredients, and some companies use double planetary vacuum mixers and ordinary single-blade mixers in conjunction; [0003] The wet batching process in the prior art is as follows: (1) Glue preparation: first add the solvent and the binder into the stirring tank, first stir at low speed for 10-20 minutes, turn on the scraping wall; then stir at high speed for 3.5 hours. (2) Add conductive agent: add conductive agent to the glue and stir at low speed for 10-20 minutes, turn on the scraping...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01F3/12B01F7/24B01F7/26B01F7/30B01F15/00B01F15/06H01M4/04B01F27/93
CPCH01M4/04B01F23/511B01F23/53B01F27/074B01F27/2322B01F27/191B01F27/922B01F27/93B01F27/951B01F35/2115B01F2035/98B01F35/92Y02E60/10
Inventor 王建红
Owner 广州云通锂电池股份有限公司
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