A kind of preparation method of fireproof glass
A technology of fireproof glass and glass, which is applied in the field of glass preparation and fireproof glass preparation, and can solve the problems of low adhesion, poor anti-aging performance and poor compatibility of fireproof liquid
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Embodiment 1
[0056] 1. Prepare fireproof liquid
[0057] 1-1) Prepare raw materials according to the following weight ratio (g)
[0058]
[0059] 1-2) Pour the raw materials potassium nitrate, cesium nitrate, Swiss seven-eight, methacrylic acid, acetone, and table salt into a plastic container filled with water in sequence, stir with an electric stirrer, and perform mixing treatment, wherein the stirring rate is 120rpm ( Usually 60-120rpm); stirring time is 1.5h;
[0060] 1-3) Stir and mix the mixed solution for 1.5 hours, and place it still at a temperature of 25° C. to allow it to fully fuse with each other and undergo a chemical reaction. After standing for 48 hours, the glass fireproof composition liquid is obtained.
[0061] 2. Replacement treatment
[0062] 2-1) Evenly spray the fireproof composition for glass on the surface of float glass with a thickness of 12mm, spray evenly on both sides of the glass, spray 12g (usually 10-15g) fireproof composition per square meter of glass...
Embodiment 2
[0080] 1. Prepare fireproof liquid
[0081] Same as Example 1
[0082] 2. Replacement treatment
[0083] Except for the thickness of the float glass which is 8mm, the spraying amount of the fireproof composition is 10g / m 2 , except that all the other are identical with embodiment 1;
[0084] 3. Cleaning and drying
[0085] Same as Example 1
[0086] 4. Tempering treatment
[0087] Except the preheating temperature in step 4-1) is 475°C; the glass reciprocates in the furnace at a speed of 80-300mm / s, and the preheating is 260s; the top hot air convection intensity: within the convection heating time interval of 1% to 50% (that is, from the time when the glass enters the tempering furnace to the 130s after entering), the convective pressure intensity of the top hot air is 3.6bar; the convective pressure of the top hot air is 50% to 70% of the convective heating time interval (that is, from the 130s to 182s after entering the tempering furnace). The strength is uniformly re...
Embodiment 3
[0092] 1. Prepare fireproof liquid
[0093] 1-1) Prepare raw materials according to the following weight ratio (g)
[0094]
[0095] 1-2) Pour the raw materials potassium nitrate, cesium nitrate, Swiss seven-eight, methacrylic acid, acetone, and salt into a plastic container filled with water in sequence, and use an electric stirrer to stir for mixing treatment, wherein the stirring rate is 100rpm ( Usually 60-120rpm); Stirring time is 2h;
[0096] 1-3) Stir and mix the mixed solution for 2 hours, and place it under the temperature condition of 25°C for sufficient mutual fusion and oxidation and reduction reactions to occur. After standing for 50 hours, the glass fireproof liquid is obtained.
[0097] 2. Replacement treatment
[0098] 2-1) Evenly spray the fireproof composition for glass on the surface of float glass with a thickness of 15mm, spray evenly on both sides of the glass, spray 15g (usually 10-15g) fireproof composition per square meter of glass surface;
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