Fluorescent material for electronic kinescope and preparation method thereof
A fluorescent material and a useful technology, applied in the directions of luminescent materials, chemical instruments and methods, can solve the problem of reducing the brightness of fluorescent materials, and achieve the effects of improving display effect, high fluorescence and convenient operation.
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Embodiment 1
[0017] A fluorescent material for an electronic picture tube, composed of Y 2 o 3 、Eu 2 o 3 , S, Na 2 CO 3 , NH 4 h 2 PO 4 and BaCl 2 2H 2 O is prepared, and its preparation method comprises the following steps:
[0018] (1) Preparation of single-phase fluorescent material: 150-200 parts of Y 2 o 3 , 15-20 Eu 2 o 3 , 150-200 parts of S, 250-350 parts of Na 2 CO 3 and 50-80 parts of NH 4 h 2 PO 4 Mix the mixture evenly, put the mixture into an alumina corundum clamp pot and heat it at 900-1100 degrees Celsius for 2-4 hours, wash the mixture with distilled water after cooling and dry it with a centrifuge to prepare Y 2 o 2 S: Eu mixed fluorescent material;
[0019] (2) single-phase fluorescent material grinding: the Y prepared in step (1) 2 o 2 S: Eu mixed fluorescent material and 400-500 parts of alumina corundum beads with a radius of 2-3 mm, 10-20 parts of BaCl 2 2H 2 0 mixed, and put into the alumina ceramic roller ball mill tank and carry out ball ...
Embodiment 2
[0022] A fluorescent material for an electronic picture tube, composed of Y 2 o 3 , Eu, Eu 2 o 3 and BaF 2 and BaCl 2 2H 2 O is prepared, and its preparation method comprises the following steps:
[0023] (1) Preparation of single-phase fluorescent material: according to parts by weight, 150 to 200 parts of Y 2 o 3 , 8 to 12 parts of Eu, 3 to 5 parts of Eu 2 o 3 , 25-35 parts of BaF 2 After mixing evenly, put the mixture into an alumina corundum clamp pot and heat it at 1300-1400 degrees Celsius for 2-4 hours. After cooling, wash the mixture with distilled water and dry it with a centrifuge to prepare Y 2 o 3 : Eu mixed fluorescent material;
[0024] (2) single-phase fluorescent material grinding: the Y prepared in step (1) 2 o 3 : Eu mixed fluorescent material and 400-500 parts of alumina corundum beads with a radius of 2-3 mm, 10-20 parts of BaCl 2 2H 2 0 mixed, and put into the alumina ceramic roller ball mill tank and carry out ball milling at a speed of 12...
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