Porous fiber, absorbing material, and purifying column
An adsorption material and porous technology, applied in the field of purification columns, can solve the problems of reduced spinning stability and achieve the effect of efficient adsorption
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Embodiment 1
[0180] [Production of porous fibers]
[0181] With mass average molecular weight being 400,000 syndiotactic PMMA (hereinafter referred to as syn-PMMA) 31.7 mass parts, mass average molecular weight being 1,400,000 syn-PMMA31.7 mass parts, mass average molecular weight being 500,000 isotactic Construct PMMA (hereinafter referred to as iso-PMMA) 16.7 mass parts, the molecular weight that comprises 1.5mol% p-styrene sulfonate sodium is the PMMA copolymer 20 mass parts of 300,000 mass parts and dimethyl sulfoxide 376 mass parts mix, at 110 ℃ After stirring for 8 hours, a spinning dope was prepared. The obtained spinning dope had a viscosity of 1,880 poise at 92°C. The spinning dope that obtains is with the speed of 1.1g / min from the nozzle that is kept at 92 ℃ (for Figure 6 The shape shown and the size shown in Table 1) were discharged into the air, and after traveling 380 mm in the air, they were introduced into a coagulation bath and passed through the bath to obtain solid fi...
Embodiment 2
[0184] In addition to using as Figure 7 Fibers were produced under the same conditions as in Example 1, except for the nozzles having the shapes shown and discharge ports having the dimensions shown in Table 1. The results are shown in Tables 1 and 2.
Embodiment 3
[0186] In addition to using as Figure 8 Fibers were produced under the same conditions as in Example 1, except for the nozzles having the shapes shown and discharge ports having the dimensions shown in Table 1. The results are shown in Tables 1 and 2.
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