A kind of regeneration method of microchannel reactor Fischer-Tropsch synthesis catalyst
A microchannel reactor, Fischer-Tropsch synthesis technology, applied in catalyst regeneration/reactivation, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problems of high material consumption and large energy consumption in the regeneration process, and achieve good performance. , performance recovery, the effect of avoiding damage
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Embodiment 1
[0034] Such as figure 1 As shown, the microchannel reactor 11 comprises 8 layers of reaction channels 12 arranged side by side and 9 layers of heat transfer medium channels 13 arranged side by side, each reaction channel is 10 mm wide, 1 mm high, and 100 mm long, and each layer has 4 reaction channels 12 . Each heat conduction medium channel has a width of 10 mm, a height of 1 mm, and a length of 100 mm, and each layer has six heat conduction medium channels 13 . The reaction channel 12 and the heat transfer medium channel 13 intersect at 90°. The cobalt-based supported Fischer-Tropsch synthesis catalyst is loaded in the reaction channel 12 .
[0035] The preparation process of the cobalt-based supported Fischer-Tropsch synthesis catalyst used in the present embodiment is as follows: get alumina powder, add distilled water dropwise to incipient wetness, write down the volume of consumed water, then press Co content (oxide) 27% by weight % calculation, a cobalt nitrate impreg...
Embodiment 2
[0043] Such as figure 2 As shown, the microchannel reactor 21 comprises 8 layers of reaction channels 22 arranged side by side and 9 layers of heat transfer medium channels 23 arranged side by side, each reaction channel 22 is 20 mm wide, 1 mm high, and 100 mm long, and each layer has 3 reaction channels 22 . Each heat conduction medium channel 23 has a width of 10 mm, a height of 1 mm, and a length of 100 mm, and each layer has six heat conduction medium channels 23 . The reaction channel 22 and the heat transfer medium channel 23 intersect at 90°. A catalyst support coated with a cobalt-based supported Fischer-Tropsch synthesis catalyst is loaded in the reaction channel 22 .
[0044] The cobalt-based Fischer-Tropsch synthesis catalyst used in this example is a coated monolithic catalyst, and the preparation process is as follows: the cobalt-based supported catalyst is coated on a treated corrugated stainless steel support body, the support body is 18 mm wide, 0.8 mm high,...
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