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An indoor evaluation device and evaluation method for defoamers used in oilfield produced fluids

A technology for indoor evaluation and production of liquid, applied in measuring devices, instruments, scientific instruments, etc., can solve the problems of long evaluation cycle, unsuitable defoamer evaluation, unfavorable product development and promotion, etc., to achieve high accuracy and safety. Good performance and small footprint

Active Publication Date: 2021-11-02
CHINA NAT OFFSHORE OIL CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the different foaming systems and foaming conditions, the current relevant standards are not suitable for the evaluation of defoamers in the process of crude oil extraction
However, the absence of indoor evaluation devices and evaluation methods for defoamers used in oilfield production fluids has led to the current on-site evaluation of platforms for product performance testing, and the evaluation cycle is too long, which is not conducive to product development and promotion.

Method used

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  • An indoor evaluation device and evaluation method for defoamers used in oilfield produced fluids
  • An indoor evaluation device and evaluation method for defoamers used in oilfield produced fluids
  • An indoor evaluation device and evaluation method for defoamers used in oilfield produced fluids

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] (1) Add 500mL of oilfield output fluid from Lvda 5-2 oilfield in Bohai Sea to the high-temperature and high-pressure stirring reactor 1, and seal the high-temperature and high-pressure stirring reactor 1 to ensure that the inlet valve 9 and exhaust of the high-temperature and high-pressure stirring reactor 1 The gas valve 11 is in an open state, and the discharge valve 14 is in a closed state. Add 50 mg of the defoamer sample to be tested into the glass measuring cylinder 5, place the glass measuring cylinder 5 directly below the drain pipe 13 of the high temperature and high pressure stirring reactor 1, and turn on the powerful searchlight 7;

[0043] (2) Open the vacuum pump 2, vacuumize the high temperature and high pressure stirred reactor 1 through the exhaust valve 11, until the pressure gauge 12 shows that the internal pressure of the high temperature and high pressure stirred reactor 1 is -0.09MPa, close the exhaust valve 11 and the vacuum pump 2 in turn;

[004...

Embodiment 2

[0056] (1) Add 500mL of oilfield output fluid from Bohai Jinzhou 9-3 oilfield into the high-temperature and high-pressure stirred reactor 1, and seal the high-temperature and high-pressure stirred reactor 1 to ensure that the inlet valve 9 and exhaust of the high-temperature and high-pressure stirred reactor 1 The valve 11 is in an open state, and the discharge valve 14 is in a closed state. Add 15 mg of the defoamer sample to be tested into the glass measuring cylinder 5, place the glass measuring cylinder 5 directly below the drain pipe 13 of the high-temperature and high-pressure stirring reactor 1, and turn on the powerful searchlight 7;

[0057] (2) Open the vacuum pump 2, vacuumize the high temperature and high pressure stirred reactor 1 through the exhaust valve 11, until the pressure gauge 12 shows that the internal pressure of the high temperature and high pressure stirred reactor 1 is -0.1MPa, close the exhaust valve 11 and the vacuum pump 2 in turn;

[0058] (3) Ope...

Embodiment 3

[0070] (1) Add 500mL of oilfield output fluid from the Bozhong 28-2S oilfield in the Bohai Sea to the high-temperature and high-pressure stirred reactor 1, and seal the high-temperature and high-pressure stirred reactor 1 to ensure that the inlet valve 9 and exhaust of the high-temperature and high-pressure stirred reactor 1 The gas valve 11 is in an open state, and the discharge valve 14 is in a closed state. Add 20 mg of the defoamer sample to be tested into the glass measuring cylinder 5, place the glass measuring cylinder 5 directly below the drain pipe 13 of the high temperature and high pressure stirring reactor 1, and turn on the powerful searchlight 7;

[0071] (2) Open the vacuum pump 2, vacuumize the high temperature and high pressure stirred reactor 1 through the exhaust valve 11, until the pressure gauge 12 shows that the internal pressure of the high temperature and high pressure stirred reactor 1 is -0.1MPa, close the exhaust valve 11 and the vacuum pump 2 in turn...

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Abstract

The invention belongs to the technical field of chemical defoaming, and discloses an indoor evaluation device and evaluation method of a defoamer for oilfield output fluid. The evaluation device is composed of a foaming device and a detection device, wherein the foaming device mainly includes high-temperature and high-pressure stirring Reaction kettle, vacuum pump, standard gas cylinder, high-pressure gas cylinder connection pipeline, detection device mainly includes glass measuring cylinder and powerful searchlight; evaluation method is to add measured oilfield output fluid into the closed reaction kettle, blow in quantitative standard gas, Stir and foam under the set temperature and pressure, then discharge the foaming liquid into a glass measuring cylinder filled with defoaming agent, record the time for the foaming liquid to disappear, and judge the performance of the defoaming agent. The evaluation device of the present invention has low investment and a small floor space, and can complete the entire performance detection process of the defoamer for crude oil output liquid in the laboratory fume hood, with high safety; the evaluation method is verified by comparison between indoor evaluation and field application, The test results have high accuracy and good repeatability.

Description

technical field [0001] The invention belongs to the technical field of chemical defoaming, and in particular relates to an indoor evaluation device and evaluation method of a defoamer, in particular to an indoor evaluation device and evaluation method of a defoamer for oilfield output liquid. Background technique [0002] When the oilfield production fluid is produced from the oil well, the associated gas originally dissolved in the crude oil is gradually separated from the crude oil due to the pressure drop and temperature change. If the gas in the crude oil cannot be removed quickly and completely, the liquid level measurement of the separator will be inaccurate after the oilfield output liquid enters the separator, which will cause fluctuations in the entire production process. Filling crude oil defoamer is an essential chemical additive for stable production in oilfields, and domestic and foreign standards for performance testing of defoamers mainly include: GB / T 26527-2...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N33/00
CPCG01N33/00
Inventor 胡廷郭海军陆原魏强程艳李羽张颖田立峰
Owner CHINA NAT OFFSHORE OIL CORP