Preparation of high-protection composite material based on TPV base material and application of high-protection composite material in high-flexibility flexible cable products
A composite material, protective technology, applied in rubber insulators, organic insulators, etc., can solve the problems of short service life, poor cable flexibility, inconvenient use, etc.
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Embodiment 1
[0025] Embodiment one: a kind of composite material preparation based on TPV base material protective property, comprises the following steps:
[0026] 1) First take several parts of maleic anhydride;
[0027] 2) Add several parts of maleic anhydride to EPDM for grafting reaction to obtain EPDM-g-MA with a grafting rate of 1-3%. The grafting reaction includes pre-mixing EPDM, free radical initiators and additives and adding them to In the internal mixer, when EPDM is completely plasticized, add 6wt% MAH based on EPDM in two times, banbury at 160°C for 10min, wash and filter to obtain EPDM-g-MAH;
[0028] 3) Add PA6 and 0.3wt% triethylamine based on PA6 to phenol, and heat to 140°C to completely dissolve the solid;
[0029] 4) Then add the xylene solution dissolved in EPDM-g-MAH into the container containing the phenol mixture, and keep it warm for 9 hours; after cooling to room temperature, pour the obtained reaction material into dimethylformamide and let it settle for 1 -2...
Embodiment 2
[0038] Embodiment two: a kind of composite material preparation based on TPV base material protective property, comprises the following steps:
[0039] 1) First take several parts of maleic anhydride;
[0040] 2) Add several parts of maleic anhydride to EPDM for grafting reaction to obtain EPDM-g-MA with a grafting rate of 1-3%. The grafting reaction includes pre-mixing EPDM, free radical initiators and additives and adding them to In the internal mixer, when EPDM is completely plasticized, add 7wt% MAH based on EPDM twice, banbury at 170°C for 12min, wash and filter to obtain EPDM-g-MAH;
[0041] 3) Add PA6 and 0.4wt% triethylamine based on PA6 to phenol, and heat to 150°C to completely dissolve the solid;
[0042] 4) Then add the xylene solution dissolved in EPDM-g-MAH into the container containing the phenol mixture, and keep it warm for 10 hours; after cooling to room temperature, pour the obtained reaction material into dimethylformamide and let it settle for 1.5 h, filte...
Embodiment 3
[0051] Embodiment three: a kind of composite material preparation based on TPV base material protective property, comprises the following steps:
[0052] 1) First take several parts of maleic anhydride;
[0053] 2) Add several parts of maleic anhydride to EPDM for grafting reaction to obtain EPDM-g-MA with a grafting rate of 3%. The grafting reaction includes pre-mixing EPDM, free radical initiators and additives and then adding them to the banburying In the machine, when EPDM is completely plasticized, add 8wt% MAH based on EPDM twice, banbury at 180°C for 15min, wash and filter to obtain EPDM-g-MAH;
[0054] 3) Add PA6 and 0.5wt% triethylamine based on PA6 to phenol, and heat to 160°C to completely dissolve the solid;
[0055] 4) Then add the xylene solution dissolved in EPDM-g-MAH into the container containing the phenol mixture, and keep it warm for 12 hours; after cooling to room temperature, pour the obtained reaction material into dimethylformamide and let it settle fo...
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