Polyimide precursor composition and method for producing polyimide film using the same
A technology of polyimide and composition, applied in the field of display devices, can solve problems such as coating surface defects, and achieve the effect of good transmittance and surface characteristics
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Embodiment 1
[0041] [Example 1] Preparation of polyimide precursor composition :
[0042] In a mixed solvent of 529.2 g of 3-methoxy-N,N-dimethylpropanamide (M3DMPA) and N,N-dimethylpropanamide (DMPA) at a ratio of 1:9 by weight After completely dissolving 21.62g (0.2mol) of p-phenylenediamine (PPDA) at room temperature, add 58.84g (0.2mol) of 3,3',4,4'-biphenyltetracarboxylic dianhydride (BPDA) to carry out The reaction was completed after stirring for 18 hours, and a composition containing 15 parts by weight of polyamic acid (polyimide precursor) was obtained with respect to 100 parts by weight of the mixed solvent. In order to confirm that polymerization proceeds smoothly and whether thin film formation is possible, the viscosity of the composition was detected using a Brookfield viscometer, and the obtained polyamic acid composition had a viscosity of 13500 cps.
Embodiment 2
[0043] [Example 2] Preparation of polyimide precursor composition :
[0044] The mixing ratio of 3-methoxy-N,N-dimethylpropionamide (M3DMPA) and N,N-dimethylpropionamide (DMPA) is 3:7, except that, by the same method as in Example 1 The method obtained polyamic acid (polyimide precursor) composition. The obtained polyamic acid composition had a viscosity of 13000 cps.
Embodiment 3
[0045] [Example 3] Preparation of polyimide precursor composition :
[0046] The mixing ratio of 3-methoxy-N,N-dimethylpropionamide (M3DMPA) and N,N-dimethylpropionamide (DMPA) is 5:5, except that, by the same method as in Example 1 The method obtained polyamic acid (polyimide precursor) composition. The obtained polyamic acid composition had a viscosity of 12500 cps.
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