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Comprehensive extracting method of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide and applications of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide

A polysaccharide and comprehensive extraction technology of Polygonatum chinensis, applied in the field of spices and cigarettes, can solve the problems of open system, high temperature and humidity, unfavorable by-product extraction, etc., and achieve the effects of mild conditions and good aroma fidelity.

Inactive Publication Date: 2019-03-01
YUNNAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

At present, the extraction of Polygonatum volatile oil mostly adopts the steam distillation method, which is a traditional method of extracting essential oils, which has the problems of open system, high energy consumption, high temperature and humidity, etc., which may easily cause thermal instability in essential oils and by-products. Destruction, on the one hand affects the yield and quality of essential oils, on the other hand is not conducive to the subsequent extraction of by-products
[0006] At present, Rhizoma Polygonatum is mainly used in food and traditional Chinese medicine, etc., and there are no relevant reports on the preparation method of Polygonatum volatile oil and polysaccharide comprehensive extraction and the application of corresponding extracts in tobacco

Method used

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  • Comprehensive extracting method of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide and applications of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide
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  • Comprehensive extracting method of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide and applications of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide

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Embodiment 1

[0033] The comprehensive extraction method of Polygonatum volatile oil and Polygonatum polysaccharide of the present embodiment comprises the following steps:

[0034] (1) Raw material preparation: Wash and remove impurities from the fresh sealwort, slice it, and then pre-cool it at -10°C for 12 hours, vacuum freeze-dry it to a state with a moisture content of 10%, and crush it so that the particles can pass through 20 Mesh screen;

[0035] (2) Supercritical CO 2 Fluid extraction: the Polygonatum granules of step (1) are subjected to supercritical CO 2 Fluid extraction, extraction temperature 40 DEG C, extraction pressure 25Mpa, entrainer (dehydrated alcohol) is 8% of raw material weight, static extraction 3h, collect Rhizoma Polygonatum residue and Polygonatum volatile oil from extracting kettle and separating kettle respectively. The volatile oil is used for later use, and the residue is used for the extraction of Polygonatum polysaccharide;

[0036] (3) Enzyme treatment:...

Embodiment 2

[0039] The comprehensive extraction method of Polygonatum volatile oil and Polygonatum polysaccharide of the present embodiment comprises the following steps:

[0040] (1) Raw material preparation: Fresh Polygonatum is washed and removed and sliced, then pre-cooled at -8°C for 18 hours, vacuum freeze-dried to a state with a moisture content of 12%, and crushed so that the particles can pass through 40 Mesh screen;

[0041] (2) Supercritical CO 2 Fluid extraction: the Polygonatum granules of step (1) are subjected to supercritical CO 2Fluid extraction, extraction temperature 50 ℃, extraction pressure 30Mpa, entrainer (dehydrated alcohol) is 12% of raw material weight, static extraction 2h, collect Rhizoma Polygonatum residue and Rhizoma Rhizoma Polygonatum volatile oil from extraction kettle and separating kettle respectively. The volatile oil is used for later use, and the residue is used for the extraction of Polygonatum polysaccharide;

[0042] (3) Enzyme treatment: Polyg...

Embodiment 3

[0047] The comprehensive extraction method of Polygonatum volatile oil and Polygonatum polysaccharide of the present embodiment comprises the following steps:

[0048] (1) Raw material preparation: Fresh Polygonatum is washed and removed and sliced, then pre-cooled at -4°C for 24 hours, then vacuum freeze-dried to a state with a moisture content of 8%, and crushed so that the particles can pass 60 Mesh screen;

[0049] (2) Supercritical CO 2 Fluid extraction: the Polygonatum granules of step (1) are subjected to supercritical CO 2 Fluid extraction, extraction temperature 60 DEG C, extraction pressure 20Mpa, entrainer (dehydrated alcohol) is 15% of raw material weight, static extraction 1.5h, collect Rhizoma Polygonatum residue and Polygonatum volatile oil from extraction kettle and separating kettle respectively. The volatile oil is used for later use, and the residue is used for the extraction of Polygonatum polysaccharide;

[0050] (3) Enzyme treatment: Polygonatum residu...

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Abstract

The invention discloses a comprehensive extracting method of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide and applications of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide. According to the comprehensive extracting method of rhizoma polygonati volatile oil and rhizoma polygonati polysaccharide, the volatile oil and polysaccharide are extracted sequentially through supercritical CO2 fluid extraction and enzyme treatment by adopting the same raw material, namely, rhizoma polygonati as the basis. The method comprises the following steps: (1) preparing for the raw material; (2) carrying out supercritical CO2 fluid extraction to obtain rhizoma polygonati volatile oil; (3) carrying out enzyme treatment; and (4) extracting and preparing the rhizomapolygonati polysaccharide. According to the technical scheme, through the comprehensive extracting method, rhizoma polygonati polysaccharide is extracted by adopting the rhizoma polygonati residue obtained after extracting of volatile oil as the raw material, meanwhile, the extracting of the rhizoma polygonati volatile oil has no influences on the follow-up extracting of polysaccharide, and thusthe rhizoma polygonati resource is sufficiently utilized. In addition, the rhizoma polygonati volatile oil provided by the invention is prepared into burst beads, the burst beads are compounded to cigarette filter sticks, and then the purpose of supplementing, enriching, and promoting or transferring cigarette perfume is achieved; and after the rhizoma polygonati polysaccharide provided by the invention is added to tobacco shreds, the moistening feeling of the oral cavity can be improved, the smoke is enabled to be mellow and full, and the comfort level of the sense organ is improved.

Description

technical field [0001] The invention belongs to the technical field of spices and cigarettes, and in particular relates to a comprehensive extraction method of Polygonatum volatile oil and Polygonatum polysaccharide and its application. Background technique [0002] Increasing flavor and moisturizing is an important foundation and guarantee for building the core technology of Chinese-style cigarettes and forming the characteristics of cigarette products. Exploring characteristic natural plant flavors, extracting and separating the aroma and moisturizing components from natural plants and combining them with tobacco aroma and moisturizing properties is an important solution for increasing the flavor and moisturizing properties of cigarette products and improving the overall quality. [0003] Polygonatum Polygonatum is a perennial herb of the genus Polygonatum in the family Liliaceae, including Polygonatum Polygonatum, Polygonatum Polygonatum and Polygonatum Polyflora. It is ...

Claims

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Application Information

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IPC IPC(8): A24B15/30
CPCA24B15/303
Inventor 李娟吴恒张克勤
Owner YUNNAN UNIV
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