Plugging agent, and preparation method and application thereof
A technology of plugging agent and curing agent, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., to achieve the effects of resisting erosion, reducing economic losses, and improving strength and success rate
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[0059] In a second aspect, the embodiments of the present invention provide a method for preparing the above-mentioned leakage stoppage agent, the preparation method comprising the following steps:
[0060] Step 1: The mica, walnut shells, mineral fibers, and quartz sand are respectively washed with water, pickled, soaked in a coupling agent, and dried to obtain pre-mica, pre-walnut shells, pre-mineral fibers, and Front quartz sand.
[0061] Wherein, the process of washing mica, walnut shells, mineral fibers, and quartz sand in step 1 is: soak mica, walnut shells, mineral fibers, and quartz sand with clear water for 2 to 3 hours to remove the adsorbed Impurities such as clay on mica surface, walnut shell surface, mineral fiber surface and quartz sand surface.
[0062] In step 1, the process of pickling the washed mica, walnut shells, mineral fibers and quartz sand is as follows: soak the above washed mica, walnut shells, mineral fibers with 0.01%-0.05% dilute sulfuric acid so...
Embodiment 1
[0086] This embodiment provides a self-consolidating material whose formulation is as follows:
[0087] 67 parts by weight of thermoplastic phenolic resin, 32.9 parts by weight of hexamethylenetetramine, and 0.1 part by weight of calcium stearate.
Embodiment 2
[0089]This embodiment provides a self-consolidating material whose formulation is as follows:
[0090] 83 parts by weight of thermoplastic phenolic resin, 16.6 parts by weight of hexamethylenetetramine, and 0.4 parts by weight of calcium stearate.
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