A kind of multi-layer composite sealing gasket and preparation method thereof
A sealing gasket and multi-layer composite technology, which is applied in the direction of engine sealing, mechanical equipment, non-polymer organic compound adhesives, etc., can solve the problems of wear resistance, aging resistance, poor rebound sealing performance, and heat resistance. Large difference in performance and aging resistance, poor mechanical strength and pressure resistance, etc., to achieve the effect of low equipment dependence, excellent wear resistance, and high mechanical strength
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Embodiment 1
[0028] A multi-layer composite sealing gasket comprises a surface layer, an adhesive layer, a core layer, an adhesive layer, and a surface layer sequentially from top to bottom.
[0029] The core layer is preferably a stainless steel sheet; the surface layer includes the following components by weight: 30 parts of polyisoprene, 20 parts of nitrile rubber, 1 part of 2-(trimethoxysilyl) ethanethiol, 1 part of diethylamine, 30 parts of chlorosulfonated polyethylene, 20 parts of fluorine-containing silicon triazine-based cyanoethyl acrylate copolymer, 15 parts of cement, and 10 parts of coal powder.
[0030] The preparation method of the fluorine-containing silicon triazine-based cyanoethyl acrylate copolymer comprises the following steps: 200 g of cyanoethyl acrylate, 100 g of 1,2,2-trifluorovinyl triphenylsilane, 2,4- Dissolve 100g of diamino-6-vinyl-S-triazine and 2g of azobisisobutyronitrile in 800g of dimethyl sulfoxide, mix well, and bubble with nitrogen gas for 25min, then ...
Embodiment 2
[0036] A multi-layer composite sealing gasket comprises a surface layer, an adhesive layer, a core layer, an adhesive layer, and a surface layer sequentially from top to bottom.
[0037] The core layer is preferably a stainless steel sheet; the surface layer includes the following components by weight: 33 parts of polyisoprene, 23 parts of nitrile rubber, 2 parts of 2-(trimethoxysilyl) ethanethiol, 2 parts of diethylamine, 33 parts of chlorosulfonated polyethylene, 23 parts of fluorine-containing silicon triazine-based cyanoethyl acrylate copolymer, 17 parts of cement, and 11 parts of coal powder.
[0038] The preparation method of the fluorine-containing silicon triazine-based cyanoethyl acrylate copolymer comprises the following steps: 200 g of cyanoethyl acrylate, 100 g of 1,2,2-trifluorovinyl triphenylsilane, 2,4- 100g of diamino-6-vinyl-S-triazine and 2.5g of azobisisoheptanonitrile were dissolved in 850g of N,N-dimethylformamide. After reacting at ℃ for 10.5 hours, the ...
Embodiment 3
[0044] A multi-layer composite sealing gasket comprises a surface layer, an adhesive layer, a core layer, an adhesive layer, and a surface layer sequentially from top to bottom.
[0045] The core layer is preferably a stainless steel sheet; the surface layer includes the following components in parts by weight: 35 parts of polyisoprene, 26 parts of nitrile rubber, 3 parts of 2-(trimethoxysilyl) ethanethiol, 3 parts of diethylamine, 35 parts of chlorosulfonated polyethylene, 26 parts of fluorine-containing silicon triazine-based cyanoethyl acrylate copolymer, 17 parts of cement, and 13 parts of coal powder.
[0046] The preparation method of the fluorine-containing silicon triazine-based cyanoethyl acrylate copolymer comprises the following steps: 200 g of cyanoethyl acrylate, 100 g of 1,2,2-trifluorovinyl triphenylsilane, 2,4- Dissolve 100g of diamino-6-vinyl-S-triazine and 3g of dimethyl azobisisobutyrate in 1000g of N-methylpyrrolidone. After reacting for 11.5 hours, the pr...
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