A kind of two-component silicone structural adhesive for solar thermal power generation and preparation method thereof
A photothermal power generation, two-component technology, applied in the direction of adhesives, polymer adhesive additives, non-polymer adhesive additives, etc., can solve the problems of reduced bonding strength, reduced cross-linking density of sealing materials, etc., to achieve Effects of improving tensile bond strength, increasing crosslink density, and improving moisture and heat aging resistance
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Embodiment 1
[0053] A component preparation
[0054] 20 parts of α, ω-dihydroxypolydimethylsiloxane with a viscosity of 700mPa·s, 80 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 20000mPa·s, 20 parts of a viscosity of 500mPa ·S polydimethylsiloxane, 30 parts of nano-active calcium carbonate, 50 parts of heavy calcium carbonate, and 5 parts of fumed white carbon black are uniformly dispersed and mixed under vacuum to prepare component A.
[0055] B component preparation
[0056] 30 parts of pigment carbon black, 40 parts of polydimethylsiloxane with a viscosity of 500mPa·s, 20 parts of the first type of crosslinking agent, 40 parts of tetraethyl orthosilicate, 10 parts of coupling agent, 2 parts of dibutyl The base tin laurate is uniformly dispersed and mixed under vacuum to prepare the B component.
[0057] Among them, the first type of cross-linking agent adopts a cross-linking agent whose X is an ethyl group and R1 and R2 are a methyl structure, and its molecular struc...
Embodiment 2
[0063] A component preparation
[0064] Mix 10 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 700mPa·s, 100 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 20000mPa·s, 20 parts of a viscosity of 500mPa ·S polydimethylsiloxane, 100 parts of nano-active calcium carbonate, 50 parts of heavy calcium carbonate, and 2 parts of fumed white carbon black are uniformly dispersed and mixed under vacuum to prepare component A.
[0065] B component preparation
[0066] 30 parts of pigment carbon black, 40 parts of polydimethylsiloxane with a viscosity of 500mPa·s, 15 parts of first-class crosslinking agent, 40 parts of tetraethyl orthosilicate, 10 parts of coupling agent, 2 parts of dibutyl The base tin laurate is uniformly dispersed and mixed under vacuum to prepare the B component.
[0067] Among them, the first type of cross-linking agent adopts a cross-linking agent in which X is octyl, R1 and R2 are methyl structures, and its molecular structure is
...
Embodiment 3
[0073] A component preparation
[0074] 40 parts of α, ω-dihydroxypolydimethylsiloxane with a viscosity of 700mPa·s, 60 parts of α,ω-dihydroxypolydimethylsiloxane with a viscosity of 20000mPa·s, 10 parts of a viscosity of 500mPa ·S polydimethylsiloxane, 60 parts of nano-active calcium carbonate, 60 parts of heavy calcium carbonate, and 5 parts of fumed white carbon black are uniformly dispersed and mixed under vacuum to prepare component A.
[0075] B component preparation
[0076] 30 parts of pigment carbon black, 40 parts of polydimethylsiloxane with a viscosity of 500mPa·s, 20 parts of the first type of crosslinking agent, 40 parts of tetraethyl orthosilicate, 10 parts of coupling agent, 2 parts of dibutyl The base tin laurate is uniformly dispersed and mixed under vacuum to prepare the B component.
[0077] Among them, the first type of cross-linking agent adopts the cross-linking agent whose X is ethyl, R1 and R2 are ethyl structure, and its molecular structure is
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