Nano hybrid molecular compound containing multiple silicon hydrogen bonds and phenyl and application thereof
A molecular compound, silicon-hydrogen bond technology, applied in electrical components, circuits, adhesives, etc., can solve the problems of difficult production and instability of POSS, and achieve the effects of high curing efficiency, low TGA loss, and high crosslinking density.
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[0053] In some more specific embodiments, the preparation method specifically includes: after mixing octavinyloctasilsesquioxane, a compound containing at least two silicon-hydrogen bonds, a catalyst, and an organic solvent, heating to reflux for silicon-hydrogen Addition reaction generates the POSS nano-hybrid molecular compound containing multiple Si-H bonds and phenyl groups. Wherein, the organic solvent can be selected from compounds capable of dissolving octavinyl octasilsesquioxane, containing at least two silicon-hydrogen bonds, but will not dissolve octavinyl octasilsesquioxane, containing at least two A silicon-hydrogen bond compound, an organic solvent for any reaction in the catalyst, such as benzene, toluene and other common organic solvents.
[0054] Further, the conditions of the aforementioned hydrosilylation reaction can refer to literatures such as "Hydrosilylation Reaction and Research" (Journal of Shaoyang Teachers College, No. 2, 1998, p82-84).
[0055] An...
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