High-nickel type ternary material NCM811 pole piece baking method
A NCM811, ternary material technology, applied in the direction of drying solid materials without heating, drying, drying machine, etc., can solve the problems of unsatisfactory baking effect, complex process steps, and excessive moisture residue, and shorten the baking time. The effect of time, simple process steps and short baking time
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Embodiment 1
[0022] A high-nickel type ternary material NCM811 pole piece baking method, comprising the following steps:
[0023] (1) First, put the NCM811 pole piece in a stainless steel tray to stack 50 layers, and put the stainless steel tray into a vacuum oven;
[0024] (2) Vacuumize the vacuum oven to a vacuum degree of -0.10MPa, feed dry nitrogen into the vacuum oven to normal pressure, set the temperature of the vacuum oven to 95°C, heat the vacuum oven for baking, and the heating rate is 4°C / min, After the vacuum oven temperature reaches the set temperature, the NCM811 electrode piece baking time is set to 2h;
[0025] (3) Repeat step (2) once;
[0026] (4) Then evacuate the vacuum oven to a vacuum degree of -0.10MPa, set the temperature of the vacuum oven to 75°C, heat the vacuum oven for baking, and the heating rate is 3°C / min. After the temperature of the vacuum oven reaches the set temperature, The baking time of NCM811 pole piece is set to 4h;
[0027] (5) Turn off the heat...
Embodiment 2
[0029] A high-nickel type ternary material NCM811 pole piece baking method, comprising the following steps:
[0030] (1) First, put the NCM811 pole piece in a stainless steel tray to stack 100 layers, and put the stainless steel tray into a vacuum oven;
[0031] (2) Vacuumize the vacuum oven to a vacuum degree of -0.10MPa, pass dry argon gas into the vacuum oven to normal pressure, set the temperature of the vacuum oven to 100°C, heat the vacuum oven for baking, and the heating rate is 4°C / min , after the vacuum oven temperature reaches the set temperature, set the NCM811 electrode piece baking time to 2h;
[0032] (3) Repeat step (2) once;
[0033] (4) Then evacuate the vacuum oven to a vacuum degree of -0.10MPa, set the temperature of the vacuum oven to 80°C, heat the vacuum oven for baking, and the heating rate is 3°C / min. After the temperature of the vacuum oven reaches the set temperature, The baking time of NCM811 pole piece is set to 4h;
[0034] (5) Turn off the hea...
Embodiment 3
[0036] A high-nickel type ternary material NCM811 pole piece baking method, comprising the following steps:
[0037] (1) First, place the NCM811 pole piece in a stainless steel tray to stack 150 layers, and put the stainless steel tray into a vacuum oven;
[0038] (2) Vacuumize the vacuum oven to a vacuum degree of -0.10MPa, feed dry nitrogen into the vacuum oven to normal pressure, set the temperature of the vacuum oven to 105°C, heat the vacuum oven for baking, and the heating rate is 5°C / min, After the vacuum oven temperature reaches the set temperature, the NCM811 electrode piece baking time is set to 2h;
[0039] (3) Repeat step (2) once;
[0040] (4) Then vacuumize the vacuum oven to a vacuum degree of -0.10MPa, set the temperature of the vacuum oven to 85°C, heat the vacuum oven for baking, and the heating rate is 4°C / min. After the temperature of the vacuum oven reaches the set temperature, The baking time of NCM811 pole piece is set to 4h;
[0041] (5) Turn off the...
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