A kind of graphene oxide-gadolinium hydroxide composite material, preparation method and application thereof

A technology of gadolinium hydroxide and composite materials, applied in chemical instruments and methods, other chemical processes, water/sludge/sewage treatment, etc. high rate effect

Active Publication Date: 2021-12-14
MINNAN NORMAL UNIV
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  • Description
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Problems solved by technology

[0012] The invention provides a graphene oxide-gadolinium hydroxide composite material, a preparation method and its application to solve practical technical problems such as low adsorption effect

Method used

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  • A kind of graphene oxide-gadolinium hydroxide composite material, preparation method and application thereof
  • A kind of graphene oxide-gadolinium hydroxide composite material, preparation method and application thereof
  • A kind of graphene oxide-gadolinium hydroxide composite material, preparation method and application thereof

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Embodiment Construction

[0045] 1. Experimental part

[0046] 1. Main raw materials and instruments

[0047] The test material provided by the implementation of the present invention is: graphene oxide (GO) (AA, Suzhou Carbon Abundance Technology Co., Ltd.), gadolinium oxide (Gd 2 o 3 ) (AR, Sinopharm Chemical Reagent Co., Ltd.), sodium hydroxide (NaOH) (AR, Guangdong. Shantou Xilong Chemical Factory), hydrochloric acid (HCl) (AR, Xilong Science Co., Ltd.), ethanol (C 2 h 5 OH) (AR, Xilong Science Co., Ltd.), ammonium molybdate tetrahydrate ((NH 4 Mo 7 o 24 .4H 2 O) (AR, Xilong Science Co., Ltd.), potassium dihydrogen phosphate (KH 2 PO 4 ) (AR, Xilong Science Co., Ltd.), L(+)—ascorbic acid (C 6 h 8 o 6 ) (AR, Xilong Science Co., Ltd.), malachite green (C 23 h 25 ClN 2 ) (AR, Shandong West Asia Chemical Industry Co., Ltd.).

[0048] The instrument provided by the implementation of the present invention is: scanning electron microscope (SEM), X-ray diffraction spectrometer (XRD), HH-4 di...

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Abstract

The invention discloses a graphene oxide-gadolinium hydroxide composite material, a preparation method and an application thereof. The present invention prepares graphene oxide-gadolinium hydroxide composite material (Gd(OH)) by direct precipitation method and hydrothermal synthesis method 3 / GO) to adsorb and remove malachite green (MG) and phosphate ion (PO) in the solution 4 3‑ ), and Gd(OH) by SEM, FT-IR, etc. 3 The structure of the / GO composite was characterized by analyzing malachite green (MG) and phosphate ion (PO) under different conditions of pH, time, temperature and initial mass concentration. 4 3‑ ) adsorption effect was discussed, the optimal adsorption conditions were determined, and the maximum adsorption capacity of malachite green and phosphate ion was obtained by fitting the Langmuir isotherm adsorption equation to be 495mg / g and 364.8mg / g respectively, the adsorption effect is remarkable .

Description

【Technical field】 [0001] The invention belongs to the technical field of preparation of water treatment agents, and in particular relates to a graphene oxide-gadolinium hydroxide composite material, a preparation method and an application thereof. 【Background technique】 [0002] There are many wastewater treatment technologies, such as: flocculation, membrane filtration, solvent extraction, biosorption, chemical precipitation, ion exchange, reverse osmosis, electrocoagulation, sintering, electrolytic precipitation, coagulation and adsorption, etc. Among them, the adsorption method has become a widely used method for removing pollutants due to its advantages of cheap production and simple operation and treatment process. It is very important to design new adsorbents with excellent adsorption capacity. [0003] There are many kinds of adsorbents, which can be mainly divided into three categories: [0004] The first category is more common porous adsorption materials, such as ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/20B01J20/30C02F1/28C02F101/30C02F101/10
CPCB01J20/06B01J20/20C02F1/283B01J20/3078C02F2101/308C02F2101/105
Inventor 闫海刚杨怀杰蔡舒雅魏诗佳吴文炳
Owner MINNAN NORMAL UNIV
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