Multi-arm high-molecular pressure sensitive paint for aerospace and preparation method thereof
An aerospace and polymer technology, which is applied in the field of multi-arm polymer pressure-sensitive paint for aerospace and its preparation, can solve the problems of complicated preparation process, long cycle, interference, etc., and achieves fast response speed, wide application and high sensitivity Effect
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[0042] For better illustrating the present invention, facilitate understanding technical scheme of the present invention, typical but non-limiting embodiment of the present invention is as follows:
[0043] Embodiments 1-5 of the present invention each provide a multi-arm polymer pressure-sensitive paint for aerospace, and the specific preparation method of the above-mentioned pressure-sensitive paint is as follows:
[0044] (1) Synthesis of precursors:
[0045] Dissolve 0.6789g (0.005mol) of pentaerythritol in 30ml of tetrahydrofuran (THF), add 6.0714g (0.060mol) of triethylamine (Et3N), then add 13.8480g (0.060mol) of dibromoisobutyryl dropwise with a dropping funnel Bromine, stirred in ice bath for 24 hours. After the reaction, the product was subjected to suction filtration, and then the solution obtained by suction filtration was spin-dried, then dissolved in ether, extracted twice with pure water, saturated sodium bicarbonate, and pure water respectively, and then added...
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