Defoaming device for cellulose solution, and defoaming method of defoaming device

A cellulose solution and defoaming technology, which is applied in fiber treatment, spinning solution filtration, textiles and papermaking, etc., can solve the problems of large temperature changes, long time consumption, gelation, etc., to improve the efficiency of defoaming, improve the Bubble effect, avoid damage effect

Pending Publication Date: 2019-07-02
CHINESE TEXTILE ACAD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing defoaming method not only takes a long time, but also the temperature in the device changes greatly, which can easily cause gelation, resulting in uneven uniformity of the spinning solution, and the defoaming effect is not obvious, and at the same time, the removal of air bubbles cannot be guaranteed. Efficiency and spinning solution quality are extremely unfavorable for continuous and large-scale production
[0009] The above factors greatly limit the industrial development of low temperature alkali / urea cellulose fiber

Method used

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  • Defoaming device for cellulose solution, and defoaming method of defoaming device
  • Defoaming device for cellulose solution, and defoaming method of defoaming device
  • Defoaming device for cellulose solution, and defoaming method of defoaming device

Examples

Experimental program
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Effect test

Embodiment 1

[0069] Such as figure 1 As shown, the defoaming device for a cellulose solution described in this embodiment includes an outer cylinder 1 configured as the main body of the defoaming device, the bottom of the outer cylinder 1 is provided with a liquid outlet; the material cylinder 2 is configured on Inside the outer cylinder 1, the material cylinder 2 is provided with a through hole; the speed regulating device 4 is configured to drive the material cylinder 2 to perform centrifugal movement; the liquid inlet pipe 3 passes through the outer cylinder 1 to send the solution into the material In the cylinder 2; the material storage device 5 communicates with the liquid outlet at the bottom of the outer cylinder 1, and is arranged at a position lower than the outer cylinder 1; the bottom of the material storage device 5 is connected with a discharge device 6, the outlet of the present invention The feeding device 6 is a vacuum discharge pump connected to the bottom of the material ...

Embodiment 2

[0076] Such as figure 1 Shown, this embodiment is the further limitation of the above-mentioned embodiment one, a kind of defoaming device of cellulose solution described in this embodiment, comprises the above-mentioned a kind of defoaming device of cellulose solution, comprises and external The pressure control device 9 connected to the cylinder 1 and the material storage device 5, and the low-temperature cooling cycle temperature control device 10 arranged around the outer cylinder 1 and the material storage device 5, the low-temperature cooling cycle temperature control device 10 is equipped with a temperature control device Low temperature coolant circulation pump.

[0077]Further, the pressure control device 9 maintains the vacuum degree in the degassing device at an absolute pressure of 5-50KPa.

[0078] Furthermore, the temperature of the low-temperature cooling cycle temperature control device 10 is -10-20°C.

[0079] The outer cylinder 1 and the material storage de...

Embodiment 3

[0081] This embodiment is a further limitation of the second embodiment above, and the temperature of the low-temperature cooling cycle temperature control device 10 described in this embodiment is -10-10°C.

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Abstract

The invention discloses a defoaming device for a cellulose solution, and a defoaming method of the defoaming device. The defoaming device comprises an outer barrel, a material barrel, a speed regulation device, a liquid inlet pipe and a material storage device, wherein the outer barrel is configured into a main body of the defoaming device; a liquid outlet is formed in the bottom of the outer barrel; the material barrel is arranged in the outer barrel and is provided with a through hole; the speed regulation device is used for driving the material barrel to make centrifugal movement; the liquid inlet pipe passes through the outer barrel and feeds a solution into the material barrel; the material storage device is communicated with the liquid outlet formed in the bottom of the outer barrel,and is arranged at the position lower than the outer barrel; a discharge device is arranged at the bottom of the material storage device. The defoaming device, which is simple in structure and easy to operate, for the cellulose solution has the characteristics of being high in defoaming efficiency, realizing continuous defoaming, and guaranteeing the continuous proceeding of the subsequent spinning; material conveying is not affected by a defoaming process, and efficient defoaming and continuous production are carried out at the same time; furthermore, the defoaming method is good in effect;the defoaming device for the cellulose solution can be used for producing a spinning solution with good stability and evenness, and does not produce gel.

Description

technical field [0001] The invention relates to a defoaming device for cellulose solution and a defoaming method for the device. Background technique [0002] Cellulose is insoluble in common solvents. The production process of regenerated cellulose fibers based on the traditional viscose method and copper ammonia method has been gradually replaced by the emerging solvent spinning technology due to complex procedures, heavy pollution and high energy consumption. Among them, the NMMO (N-methylmorpholine oxide) solvent method, the ionic liquid method and the low-temperature alkali / urea method are more promising. The production of cellulose fibers by the NMMO solvent method has been industrialized, but due to cost factors and some reasons of the fiber itself, the expansion of the production scale of the NMMO solvent method is restricted to some extent. Although ionic liquids are good solvents for cellulose, they have the disadvantages of high solution viscosity and high dissol...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01D1/10
CPCD01D1/103
Inventor 孙玉山高敏张东吴振兴迟克栋张万勇
Owner CHINESE TEXTILE ACAD
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