A kind of graphene-plant porous composite microsphere and its preparation method and application
A technology of porous composite microspheres and graphene, which is applied in the field of cigarettes, can solve the problems of aroma substance loss, uneven release, long storage time, etc., and achieve the goal of reducing irritation and miscellaneous gas, uniform and sufficient release, and reducing harmful components Effect
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Embodiment 1
[0033] A preparation method of graphene-plant porous composite microspheres, comprising the steps of:
[0034] Step (a), after washing and removing impurities, the strawberries are crushed and processed into particles with a particle size of 2-5 mm;
[0035] Step (b), put the strawberry granules obtained in step (a) in a vacuum freeze dryer, keep it at a vacuum degree of 15-25kPa and a temperature of -40°C for 4 hours, and then raise the temperature to within 10 hours. 10 ℃, to obtain strawberry freeze-dried porous particles;
[0036] Step (c), sieving the strawberry freeze-dried porous particles prepared in step (b) to obtain strawberry freeze-dried porous particles with a size range of 1-4 mm;
[0037] In step (d), the strawberry freeze-dried porous particles obtained in step (c) are mixed with the graphene material loaded with flavors and fragrances at a mass ratio of 5:1, and a binder is added by spheronization to obtain microspheres ;
[0038] The added mass of the bin...
Embodiment 2
[0047] A preparation method of graphene-plant porous composite microspheres, comprising the steps of:
[0048] Step (a), after washing and removing impurities from the spice plant Panax notoginseng, crushing and processing it into particles with a particle size of 2-5 mm;
[0049] Step (b), put the notoginseng granules obtained in step (a) in a vacuum freeze dryer, keep it at a vacuum degree of 15-25kPa and a temperature of -20°C for 8 hours, and then raise the temperature within 25 hours to 20°C to obtain freeze-dried porous particles of notoginseng;
[0050] Step (c), sieving the notoginseng freeze-dried porous particles prepared in step (b) to obtain notoginseng freeze-dried porous particles with a size range of 1-4 mm;
[0051] In step (d), the notoginseng freeze-dried porous particles obtained in step (c) are mixed with the graphene material loaded with flavors and fragrances at a mass ratio of 20:1, and a binder is added by a spheronization process to obtain micropartic...
Embodiment 3
[0061] A preparation method of graphene-plant porous composite microspheres, comprising the steps of:
[0062] Step (a), after washing and removing impurities, the spice plants are crushed and processed into particles with a particle size of 0.2-0.5 mm;
[0063] Step (b), place the spice plant granules obtained in step (a) in a vacuum freeze dryer, keep it under the conditions of a vacuum degree of 15~25kPa and a temperature of -30°C for 6 hours, and then raise the temperature within 18 hours to 15°C to obtain freeze-dried porous particles of spice plants;
[0064] Step (c), sieving the spice plant freeze-dried porous particles prepared in step (b), to obtain blueberry plant freeze-dried porous particles with a size range of 0.08-0.2 mm;
[0065] In step (d), the 0.05-0.2 mm freeze-dried porous particles of spice plants obtained in step (c) are mixed with the graphene material loaded with flavor and fragrance in a mass ratio of 12:1, and the bonding is added by spheronization...
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