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A high-efficiency electrode for treating industrial circulating cooling water and its preparation method

A technology of circulating cooling water and electrodes, which is applied in the direction of active material electrodes, water/sewage treatment, chemical instruments and methods, etc., can solve the problems of high price, electrochemical activity, weak sterilization ability, high energy consumption, etc., and achieve sterilization ability Strong, increased reactive sites, low energy consumption

Active Publication Date: 2022-02-11
HUANENG CLEAN ENERGY RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

But its price is expensive, its electrochemical activity and bactericidal ability are not strong, and its energy consumption is high.

Method used

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  • A high-efficiency electrode for treating industrial circulating cooling water and its preparation method
  • A high-efficiency electrode for treating industrial circulating cooling water and its preparation method

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preparation example Construction

[0031] The preparation method of the high-efficiency electrode for treating industrial circulating cooling water according to the present invention comprises the following steps:

[0032] 1) Select a titanium plate and pretreat the titanium plate;

[0033] 2) the first SnCl 4 ·5H 2 O and the soluble metal salt containing Ce are dissolved in the first organic solvent, and then aged to obtain the precursor solution A;

[0034] 3) the second part of SnCl 4 ·5H 2 O, SbCl 3 and RuCl 3 Dissolved in the second part of organic solvent, and then aged to obtain precursor solution B;

[0035] 4) Apply the precursor solution A to the titanium plate obtained by step 1) in stages, wherein, after each application of the precursor solution A, it is grilled and roasted to obtain Ti / Ce-SnO 2 electrode;

[0036] 5) Brush the precursor solution B onto the Ti / Ce-SnO obtained in step 4) 2 Electrodes, wherein, after each brushing is completed, it is baked and roasted to be used for processi...

Embodiment 1

[0050] The preparation method of the high-efficiency electrode for treating industrial circulating cooling water according to the present invention comprises the following steps:

[0051] 1) Select a titanium plate and pretreat the titanium plate;

[0052] 2) the first SnCl 4 ·5H 2 O and the soluble metal salt containing Ce are dissolved in the first organic solvent, and then aged to obtain the precursor solution A;

[0053] 3) the second part of SnCl 4 ·5H 2 O, SbCl 3 and RuCl 3 Dissolved in the second part of organic solvent, and then aged to obtain precursor solution B;

[0054] 4) Apply the precursor solution A to the titanium plate obtained by step 1) in stages, wherein, after each application of the precursor solution A, it is grilled and roasted to obtain Ti / Ce-SnO 2 electrode;

[0055] 5) Brush the precursor solution B onto the Ti / Ce-SnO obtained in step 4) 2 Electrodes, wherein, after each brushing is completed, it is baked and roasted to be used for processi...

Embodiment 2

[0067] The preparation method of the high-efficiency electrode for treating industrial circulating cooling water according to the present invention comprises the following steps:

[0068] 1) Select a titanium plate and pretreat the titanium plate;

[0069] 2) the first SnCl 4 ·5H 2 O and the soluble metal salt containing Ce are dissolved in the first organic solvent, and then aged to obtain the precursor solution A;

[0070] 3) the second part of SnCl 4 ·5H 2 O, SbCl 3 and RuCl 3 Dissolved in the second part of organic solvent, and then aged to obtain precursor solution B;

[0071] 4) Apply the precursor solution A to the titanium plate obtained by step 1) in stages, wherein, after each application of the precursor solution A, it is grilled and roasted to obtain Ti / Ce-SnO 2 electrode;

[0072] 5) Brush the precursor solution B onto the Ti / Ce-SnO obtained in step 4) 2 Electrodes, wherein, after each brushing is completed, it is baked and roasted to be used for processi...

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Abstract

The invention discloses a high-efficiency electrode for treating industrial circulating cooling water and a preparation method thereof, which comprises Ti substrates, SnO 2 ‑Ce interlayer and SnO 2 ‑Sb‑Ru active layer, the electrode has the characteristics of high catalytic activity, high corrosion resistance stability, strong bactericidal ability and low energy consumption, and the preparation is relatively simple and the cost is low.

Description

technical field [0001] The invention belongs to the technical field of electrochemical water treatment, and relates to a high-efficiency electrode for treating industrial circulating cooling water and a preparation method thereof. Background technique [0002] The circulating water system is one of the indispensable energy media for the production of metallurgy, energy and chemical enterprises. With the increase of the concentration ratio of circulating cooling water, the phenomenon of microbial reproduction, fouling and corrosion will appear in the system. In order to prevent the water quality from deteriorating indefinitely, on the one hand, part of the concentrated water must be discharged to supplement the clean water, and on the other hand, sterilization, anti-scaling and anti-corrosion treatment must be carried out. At present, the chemical agent method is generally used to control the quality of circulating cooling water. This method has problems such as high chemica...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01M4/02
CPCC02F1/46109C02F2001/46142
Inventor 王广任志博张畅余智勇
Owner HUANENG CLEAN ENERGY RES INST
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