Production process for preparing lubricating oil through coffee residue oil
A production process and technology of coffee grounds, applied in the field of lubricating oil, can solve problems such as the health impact of operators, the economic benefits of wasting coffee grounds, etc., and achieve the effects of not being easy to deteriorate, cost saving, and strong anti-oxidation performance
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Embodiment 1
[0031] (1) Place the coffee grounds in a stirring dryer for drying, and grind the dried coffee grounds to a particle size of 0.1-2mm;
[0032] (2) Put the ground coffee grounds and n-hexane in a mass ratio of 1:4 into a still with a reflux device, mix evenly, and stir at 55°C for 7 hours;
[0033] (3) filtering the mixture after the n-hexane extraction in step (2) to obtain a mixed liquid, and then evaporating under reduced pressure to remove and recover the n-hexane in the mixed liquid to obtain coffee grounds oil;
[0034] (4) Transfer 1 mass part of isooctanoic acid and 500 mass parts of coffee grounds oil obtained in step (3) to a closed reactor, heat to 70°C, add 120 mass parts of potassium hydroxide, heat up to 120°C and maintain, and stir until The materials are fully mixed to obtain a melt;
[0035] (5) Lower the temperature to 45°C, and add 1000 parts by mass of coffee grounds oil obtained in step (3), 230 parts by mass of ethanol, 2300 parts by mass of diglycerin po...
Embodiment 2
[0037] (1) Place the coffee grounds in a stirring dryer for drying, and grind the dried coffee grounds to a particle size of 0.1-2mm;
[0038] (2) Put the ground coffee grounds and n-hexane at a mass ratio of 1:4 into a still with a reflux device, mix evenly, and stir at 75°C for 6 hours;
[0039] (3) filtering the mixture after the n-hexane extraction in step (2) to obtain a mixed liquid, and then evaporating under reduced pressure to remove and recover the n-hexane in the mixed liquid to obtain coffee grounds oil;
[0040] (4) Transfer 1 mass part of isooctanoic acid and 500 mass parts of coffee grounds oil obtained in step (3) to a closed reactor, heat to 70°C, add 120 mass parts of potassium hydroxide, heat up to 120°C and maintain, and stir until The materials are fully mixed to obtain a melt;
[0041] (5) Lower the temperature to 45°C, and add 1000 parts by mass of coffee grounds oil obtained in step (3), 230 parts by mass of ethanol, 2300 parts by mass of diglycerin po...
Embodiment 3
[0043] (1) Place the coffee grounds in a stirring dryer for drying, and grind the dried coffee grounds to a particle size of 0.1-2mm;
[0044] (2) Put the ground coffee grounds and n-hexane in a mass ratio of 1:4 into a still with a reflux device, mix evenly, and stir at 55°C for 9 hours;
[0045] (3) filtering the mixture after the n-hexane extraction in step (2) to obtain a mixed liquid, and then evaporating under reduced pressure to remove and recover the n-hexane in the mixed liquid to obtain coffee grounds oil;
[0046] (4) Transfer 1 mass part of isooctanoic acid and 500 mass parts of coffee grounds oil obtained in step (3) to a closed reactor, heat to 70°C, add 120 mass parts of potassium hydroxide, heat up to 120°C and maintain, and stir until The materials are fully mixed to obtain a melt;
[0047] (5) Lower the temperature to 45°C, and add 1000 parts by mass of coffee grounds oil obtained in step (3), 230 parts by mass of ethanol, 2300 parts by mass of diglycerin po...
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