Antibacterial natural silk fiber product and preparation method thereof

A technology of natural silk and fiber products, applied in the field of fiber production and processing, can solve the problems of insufficient bactericidal ability and insufficient lasting adhesion between silver atom particles and silk fibers, and achieve durable and effective antibacterial properties, strong antibacterial ability and strong adhesion. Effect

Inactive Publication Date: 2019-12-24
FUYANG AOHONG FIBER PROD CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] In the Chinese invention with the publication number CN106917266A, an antibacterial natural silk fiber product and its preparation method are provided. It uses silver salt and formic acid to reduce the silver atomic particles and make them adhere to the silk fiber, but its bactericidal ability is not enough Strong, and the adhesion between silver atomic particles and silk fibers is not durable enough

Method used

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  • Antibacterial natural silk fiber product and preparation method thereof
  • Antibacterial natural silk fiber product and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Configuration mass concentration is the formic acid solution of 80%, then in the formic acid solution, add the silver nitrate of 0.5% and the titanium tetrachloride of 0.5%, make treatment liquid after stirring slowly; Natural silk fiber is cleaned, then in 40 degree After soaking in warm water for a period of time, dry it, then put the natural silk fiber into the quaternary ammonium salt solution with a mass concentration of 45% and soak it for a period of time; immerse the processed natural silk fiber product in the treatment solution, and keep it in the dark for 1-20 minutes. 2 days; then the natural silk fiber products are washed and dried to obtain antibacterial natural silk fiber products.

Embodiment 2

[0024] Configuration mass concentration is the formic acid solution of 80%, then in the formic acid solution, add 15% silver nitrate and 15% titanium tetrachloride, make treatment liquid after stirring slowly; Natural silk fiber is cleaned, then in 40 degree After soaking in warm water for a period of time, dry it, then put the natural silk fiber into the quaternary ammonium salt solution with a mass concentration of 45% and soak it for a period of time; immerse the processed natural silk fiber product in the treatment solution, and keep it in the dark for 1-20 minutes. 2 days; then the natural silk fiber products are washed and dried to obtain antibacterial natural silk fiber products.

Embodiment 3

[0026] Configuration mass concentration is the formic acid solution of 80%, then in the formic acid solution, add 7% silver nitrate and 7% titanium tetrachloride, make treatment liquid after stirring slowly; Natural silk fiber is cleaned, then in 40 degree After soaking in warm water for a period of time, dry it, then put the natural silk fiber into the quaternary ammonium salt solution with a mass concentration of 45% and soak it for a period of time; immerse the processed natural silk fiber product in the treatment solution, and keep it in the dark for 1-20 minutes. 2 days; then the natural silk fiber products are washed and dried to obtain antibacterial natural silk fiber products.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses an antibacterial natural silk fiber product and a preparation method thereof; the preparation method comprise the steps of preparing a formic acid solution, wherein the mass concentration of the formic acid is 60-90%; then adding silver salt and inorganic titanium salt water into the formic acid solution, wherein the silver salt is one or more of silver nitrate, silver chloride, silver bromide and silver fluoride, and the inorganic titanium salt water is titanium tetrachloride; and slowly stirring to obtain a treatment solution, wherein in the treatment liquid, the massconcentration of the silver salt is 0.5-15%, and the mass concentration of the inorganic titanium salt water is 0.5-15%; cleaning natural silk fibers; then soaking the natural silk fibers in warm water for a period of time before airing; then soaking the natural silk fibers in a surfactant for a period of time, wherein the surfactant is a quaternary ammonium salt solution; soaking the treated natural silk fiber product in the treatment solution, and allowing to stand in the dark for 1-2 days; and then washing and drying the natural silk fiber product to obtain the antibacterial natural silk fiber product.

Description

technical field [0001] The invention relates to the technical field of fiber production and processing, in particular to an antibacterial natural silk fiber product and a preparation method thereof. Background technique [0002] Silk is a continuous long fiber formed by the solidification of the silk liquid secreted by cooked silkworms when they cocoon. It is also called natural silk and is a natural fiber. Humans utilized one of the first animal fibers. Silk is one of the products of ancient Chinese civilization. The Chinese laboring people invented and produced it very early. According to legend, the concubine of the Yellow Emperor Luozu first taught the people to raise silkworms. According to archaeological discoveries, about 4,700 years ago, silk was used in China to make silk threads, weave ribbons and simple silk fabrics. During the Shang and Zhou dynasties, silk was used to weave silk products such as Luo, damask, Wan, yarn, crepe, Qi, brocade and embroidery. Silkw...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/83D06M13/46D06M101/10
CPCD06M11/83D06M13/46D06M16/00D06M2101/10
Inventor 周鹤飞张蒙王艳云
Owner FUYANG AOHONG FIBER PROD CO LTD
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