Confinement growth znin in a hollow carbon nanosphere 2 the s 4 Photocatalyst and its preparation method
A photocatalyst, znin2s4 technology, applied in catalyst activation/preparation, physical/chemical process catalysts, chemical instruments and methods, etc., to achieve the effects of good photocatalytic hydrogen production stability, simple preparation method, and excellent light-driven hydrogen production activity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0039] Confined Growth ZnIn in Carbon Nano Hollow Spheres of the Invention 2 S 4 The preparation method of photocatalyst comprises the following steps:
[0040] 1a) Dissolve indium nitrate, zinc nitrate and L-cysteine in deionized water, then stir at room temperature to obtain a solution, wherein the ratio of indium nitrate, zinc nitrate, L-cysteine and deionized water For: 0.2-1.0g: 1.2-2.0g: 4.0-6.0g: 4.0-6.0g: 40-60mL;
[0041] 2a) Transfer the solution obtained in step 1a) to a polytetrafluoroethylene-lined stainless steel autoclave, heat and maintain it, then cool to room temperature, wash with deionized water and ethanol to obtain a black-green product, and then turn the black-green The product is dried to obtain the confinement growth ZnIn in microspherical carbon nano hollow spheres 2 S 4Photocatalyst (microsphere ZnIn 2 S 4 catalyst of light).
[0042] The time of stirring in step 1a) is 1-5h;
[0043] In step 2a), heat to 180-200°C and keep for 3-6h;
[...
Embodiment 1
[0061] Confined Growth ZnIn in Carbon Nano Hollow Spheres of the Invention 2 S 4 The preparation method of photocatalyst comprises the following steps:
[0062] 1a) Dissolve indium nitrate, zinc nitrate and L-cysteine in deionized water, then stir at room temperature to obtain a solution, wherein the ratio of indium nitrate, zinc nitrate, L-cysteine and deionized water For: 0.2g: 2.0g: 4.0g: 6.0g: 40mL;
[0063] 2a) Transfer the solution obtained in step 1a) to a polytetrafluoroethylene-lined stainless steel autoclave, heat and maintain it, then cool to room temperature, wash with deionized water and ethanol to obtain a black-green product, and then turn the black-green The product is dried to obtain the confinement growth ZnIn in microspherical carbon nano hollow spheres 2 S 4 catalyst of light.
[0064] The time of stirring in step 1a) is 5h;
[0065] Heating to 200°C in step 2a) and maintaining for 6h;
[0066] In step 2a), the black-green product was dried in an...
Embodiment 2
[0068] Confined Growth ZnIn in Carbon Nano Hollow Spheres of the Invention 2 S 4 The preparation method of photocatalyst comprises the following steps:
[0069] 1a) Dissolve indium nitrate, zinc nitrate and L-cysteine in deionized water, then stir at room temperature to obtain a solution, wherein the ratio of indium nitrate, zinc nitrate, L-cysteine and deionized water For: 1.0g: 1.2g: 6.0g: 4.0g: 60mL;
[0070] 2a) Transfer the solution obtained in step 1a) to a polytetrafluoroethylene-lined stainless steel autoclave, heat and maintain it, then cool to room temperature, wash with deionized water and ethanol to obtain a black-green product, and then turn the black-green The product is dried to obtain the confinement growth ZnIn in microspherical carbon nano hollow spheres 2 S 4 catalyst of light.
[0071] The time of stirring in step 1a) is 1h;
[0072] Heating to 180°C in step 2a) and maintaining for 3h;
[0073] In step 2a), the black-green product was dried in an...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More