Disperse dye and preparation process thereof
A disperse dye and preparation technology, applied in the field of dyes, can solve problems such as contamination, achieve the effects of improving surface roughness, bright color, and improving color fastness
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[0044] Preparation of dye monomer: the general formula is The compound diazotization, and the diazonium salt of this compound is coupled to obtained from above, where R 1 is chlorine or bromine, R 2 is methyl or ethyl, R 3 is methyl or ethyl.
Embodiment 1
[0047] The invention discloses a preparation process of disperse dyes, comprising the following steps:
[0048] S1, first mix the silica sol and distilled water, and adjust the pH value to 4;
[0049] S2. Then add dye monomer, 6-bromo-2,4-dinitroaniline, dispersant and disperse blue 2BLN to obtain a preliminary mixture, stir and mix at 45°C, and then grind with a sand mill to obtain a dispersion dye. The content of each component is shown in Table 1 below.
Embodiment 2
[0051] The invention discloses a preparation process of disperse dyes, comprising the following steps:
[0052] S1, first mix the silica sol and distilled water, and adjust the pH value to 5;
[0053] S2. Then add dye monomer, 6-bromo-2,4-dinitroaniline, dispersant and disperse blue 2BLN to obtain a preliminary mixture, stir and mix at 50°C, and then grind with a sand mill to obtain a dispersion dye. The content of each component is shown in Table 1 below.
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