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Preparation process of multilayer-permeability and multilayer-strength false tooth

A preparation process and denture technology, applied in the direction of dental preparations, dental prostheses, compression mold cups, etc., can solve the problems of excessive sharpness, complex process, and excessive incision, and achieve smooth and natural color, good biocompatibility, and reduced The effect of tooth preparation

Inactive Publication Date: 2020-06-30
上海美达义齿制作有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In prosthodontics, the problem of color reproduction is an important indicator that affects the aesthetics of restorations and teeth. The color of uncolored zirconia ceramics is mostly white to ivory, and the color of the prepared denture is single, which is difficult to meet the clinical requirements for complex colors sexual demands
[0003] At present, the preparation method of dental ceramics by most manufacturers of dental ceramic materials is generally to dissolve soluble rare earth salts in water or ethanol, then add zirconia powders of different permeability for stirring, and then pour them into a baking tray for drying. Then carry out ball milling and sieving to obtain small materials, and then mix the small powder materials with powders of different permeability in different proportions to obtain colored zirconia powders, and then carry out layered pressing according to the powder permeability levels, Isostatic pressing, pre-sintering, and multi-color zirconia blanks are obtained, so that the same batch of dental ceramic materials produced has only one color, and if different colors are required, the color of the powder small material should be controlled, and one color should be used The powder can only produce a single color corresponding to the produced zirconia green body. If the color is changed according to the Vita color guide, a variety of powder small materials need to be produced, so the production process is complicated and the preparation process is cumbersome.
And because its strength changes gradually, it is easy to cause the incisal end to be too hard or too sharp during the cutting and forming process, which will cause damage to the jaw teeth.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] Embodiment 1: Provide a kind of preparation technology of multi-layer transparency, multi-layer strength denture, comprise the following steps

[0042] (1) Prepare multi-layer light transmittance body: K1 (light transmittance 48%, BET 12m 2 / g) and K2 (transmittance 40%, BET25m 2 / g) The zirconia powder is mixed according to the weight ratio of 6:1, 4:1, 2:1, 1:2, 1:4, 1:6 to obtain six mixed zirconia powders of different colors, and these mixed oxidized The zirconium powder is paved layer by layer from dark to light, and then pre-pressed (pre-pressed pressure is 5MPa) to obtain a six-layer light transmittance body;

[0043] (2) Forming of multi-layer light transmittance green body: Carry out overall dry pressing (pressure of 55 MPa, holding time of 1 min) and isostatic pressing of the six-layer light transmittance green body, and then multi-layer light transmittance green body Body pre-sintering (sintering temperature is 1200 ℃, holding time is 1 hour) to obtain six-...

Embodiment 2

[0046] Embodiment 2: Provide a kind of preparation technology of multi-layer transparency, multi-layer strength denture, comprise the following steps

[0047] (1) Prepare multi-layer light transmittance body: K1 (light transmittance 48%, BET 12m 2 / g) and K2 (transmittance 40%, BET25m 2 / g) The zirconia powder is mixed according to the weight ratio of 6:1, 2:1, 1:2, 1:6 to obtain four mixed zirconia powders of different colors, and these mixed zirconia powders are changed from dark to light Sequential paving layer by layer and then pre-pressing (pre-pressing pressure is 5MPa) to obtain a four-layer light transmittance green body;

[0048] (2) Forming of multi-layer light transmittance green body: Carry out overall dry pressing (pressure of 55 MPa, holding time of 1 min) and isostatic pressing of the four-layer light transmittance green body, and then multi-layer light transmittance green body Body pre-sintering (sintering temperature is 1200 ℃, holding time is 1 hour) to obt...

Embodiment 3

[0051] Embodiment 3: provide a kind of preparation technology of multi-layer transparency, multi-layer strength denture, comprise the following steps

[0052] (1) Prepare multi-layer light transmittance body: K1 (light transmittance 48%, BET 12m 2 / g) and K2 (transmittance 40%, BET12m 2 / g) The zirconia powder is mixed according to the weight ratio of 6:1, 4:1, 2:1, 1:2, 1:4, 1:6 to obtain six mixed zirconia powders of different colors, and these mixed oxidized The zirconium powder is paved layer by layer from dark to light, and then pre-pressed (pre-pressed pressure is 5MPa) to obtain a six-layer light transmittance body;

[0053] (2) Forming of multi-layer light transmittance green body: Carry out overall dry pressing (pressure of 55 MPa, holding time of 1 min) and isostatic pressing of the six-layer light transmittance green body, and then multi-layer light transmittance green body Body pre-sintering (sintering temperature is 1200 ℃, holding time is 1 hour) to obtain six-...

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Abstract

The invention relates to the technical field of dental ceramics, in particular to a preparation process of a multilayer-permeability and multilayer-strength false tooth. The preparation method comprises the following steps: (1) mixing at least two kinds of zirconium oxide powder with different light transmittance according to different weight proportions to obtain mixed zirconium oxide powder withdifferent colors, paving the mixed zirconium oxide powder layer by layer in a sequence from dark to light, and then pre-pressing to obtain a multilayer light transmittance green body; (2) carrying out integral dry pressing and isostatic pressing molding on the multilayer light transmittance green body, presintering the multilayer light transmittance green body to obtain a multilayer zirconium oxide ceramic block, and cutting the multilayer zirconium oxide ceramic block to form a false tooth; and (3) soaking the false tooth in a staining solution, then taking out the false tooth, drying, and sintering to obtain the multilayer-permeability and multilayer-strength false tooth. The denture obtained by the method disclosed by the invention is natural and attractive in gradual change from the cutting end to the gingival end, and the strength from the cutting end to the gingival end is changed from 690-1200MPa, so that the damage to jaw teeth due to the fact that the zirconium oxide cuttingend is too hard is avoided.

Description

technical field [0001] The invention relates to the technical field of dental ceramics, in particular to a preparation process of a denture with multi-layer transparency and multi-layer strength. Background technique [0002] In prosthodontics, the problem of color reproduction is an important indicator that affects the aesthetics of restorations and teeth. The color of uncolored zirconia ceramics is mostly white to ivory, and the color of the prepared denture is single, which is difficult to meet the clinical requirements for complex colors sexual demands. [0003] At present, the preparation method of dental ceramics by most manufacturers of dental ceramic materials is generally to dissolve soluble rare earth salts in water or ethanol, then add zirconia powders of different permeability for stirring, and then pour them into a baking tray for drying. Then carry out ball milling and sieving to obtain small materials, and then mix the small powder materials with powders of d...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/48C04B35/622C04B41/87A61K6/818A61K6/15A61C13/083
CPCA61C13/083C04B35/48C04B35/622C04B41/5027C04B41/87C04B2235/5409C04B2235/656C04B2235/6567C04B2235/96C04B2235/9653C04B2235/9661C04B41/4535C04B41/0072
Inventor 韦拾庆
Owner 上海美达义齿制作有限公司
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