High-temperature-resistant antibacterial nanofiber non-woven fabric and preparation method and application thereof

A technology of nanofibers and non-woven fabrics, which is applied in fiber processing, textiles and papermaking, and fiber chemical characteristics. Low temperature and other issues, to achieve the effect of blocking and adsorbing viruses and bacteria, light weight and high air permeability

Pending Publication Date: 2020-08-04
QINGDAO UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The existing electrospun fibers and non-woven fabrics are mainly concentrated in the fields of shape control, filter materials, heat preservation and photoelectric material preparation.
At the same time, the heat-resistant temperature of most materials is low, so it is not suitable for high-temperature disinfection operations

Method used

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  • High-temperature-resistant antibacterial nanofiber non-woven fabric and preparation method and application thereof
  • High-temperature-resistant antibacterial nanofiber non-woven fabric and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] 1) Polybutene, nano-silver (bacteriostatic agent), tetrakis [β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate] pentaerythritol ester (antiaging agent 1), phosphorous acid tri( 2,4-di-tert-butylphenyl) ester (antiaging agent 2), stearic acid (antistatic agent), titanium oxide (coloring agent), sodium dodecylbenzenesulfonate (surfactant), calcium carbonate (filler) according to the prescription of table 1, blend in twin-screw extruder, granulate, make special material for non-woven fabric;

[0031] 2) Add the above-mentioned special material for non-woven fabrics into the barrel of the electrospinning equipment, control the temperature of the barrel to 200°C, set the distance between the two poles of the electrospinning equipment to 20cm, the applied voltage between the two poles to 60kV, and the spinning solution to advance at a speed of 200μL / h; the spinning environment temperature is 40°C, the spinning environment humidity is 40%, and the spinning time is 0.5h to obtai...

Embodiment 2

[0036] The polybutene / polypropylene inner alloy, Na 7 PMo 11 MnO 40 (antibacterial agent), octadecyl-3,5-bis(1,1-dimethylethyl)-4-hydroxyphenylpropionate (antiaging agent 1), tetrakis[β-(3,5- Di-tert-butyl-4-hydroxyphenyl) propionate] pentaerythritol ester (antiaging agent 2), dodecyltrimethylammonium chloride (antistatic agent), methylene blue (dyeing agent), octadecyl Sodium sulfate (surfactant) and silicon dioxide (filler) are blended in a twin-screw extruder according to the formula in Table 1, and granulated to make special materials for non-woven fabrics.

[0037] Others are the same as embodiment 1. The prepared microfiber nonwovens were tested, and the results are listed in Table 1.

Embodiment 3

[0039] Except that the butene polymer used is a polybutene / polyethylene kettle alloy, and the spinning time is 4 hours, the others are the same as in Example 2.

[0040] The prepared microfiber nonwovens were tested, and the results are listed in Table 1.

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Abstract

The invention discloses a high-temperature-resistant antibacterial nanofiber non-woven fabric and a preparation method and application thereof. The non-woven fabric is prepared from 51%-98.5% by weight of butene polymer, 0.05%-5% by weight of a bacteriostatic agent, 0.05%-5% by weight of an anti-aging agent, 0.05%-5% by weight of an antistatic agent, 0%-2% by weight of a coloring agent, 0%-2% by weight of a surfactant and 0% to 30% by weight of an inorganic filler. The non-woven fabric is formed by disorderly arranging multiple layers of superfine fibers with the diameter of 100-1000 nm, the thickness of the non-woven fabric is 5 microns to 1 centimeter, the non-woven fabric has inhibiting and killing effects on fungi, bacteria and viruses, the sterilization rate reaches 99.99%, and the virus inhibition rate reaches 99.99%. The non-woven fabric is prepared by adopting melt electrostatic spinning.

Description

technical field [0001] The invention belongs to the field of polymer superfine fiber non-woven fabrics, relates to electrospinning preparation technology, in particular to a butene polymer nanofiber non-woven fabric and its preparation method and application. Background technique [0002] High isotactic polybutene is a semi-crystalline polyolefin material with outstanding thermal creep resistance, stress cracking resistance, high heat resistance temperature, and high toughness. Polyolefin alloys (bottle alloys and physical blends) based on high isotactic polybutene not only have the advantages of polybutene, but also have the characteristics of another polyolefin. Polybutene is mainly used in pipes and can also be used in the field of film materials. [0003] Electrospinning technology is currently the most simple and effective method for preparing nanofibers, and the diameter of the prepared fibers can be between 10nm and 1000nm. In the electrospinning (electrospinning) p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D04H1/4291D04H1/728D04H3/007D04H3/02D01D5/00D01F1/10D01F6/46
CPCD01D5/0023D01F1/10D01F1/103D01F6/46D04H1/4291D04H1/728D04H3/007D04H3/02D10B2401/13D10B2505/04D10B2509/00
Inventor 邵华锋贺爱华刘晨光
Owner QINGDAO UNIV OF SCI & TECH
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