Solidification treatment method and resource application of natural gas drilling cuttings
A technology for drilling cuttings and solidification treatment, applied in fixed/solidified sludge treatment, chemical instruments and methods, sludge treatment, etc. Low cost and the effect of solving pollution problems
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Embodiment 1~ Embodiment 8
[0042] Embodiments 1 to 8 solidify the drilling cuttings according to the following steps:
[0043] (1) Pretreatment: sieve drilling cuttings to obtain cuttings samples with a particle size not greater than 5mm;
[0044] (2) Adjust the water content: use water to adjust the water content of the cuttings sample to 40% ± 2%
[0045] (3) solidification treatment: add cement, lime, fly ash and activated carbon to the rock chip sample of step (2) gained, mix and stir evenly, obtain solidified rock chip soil;
[0046] (4) Compression molding: the solidified rock debris soil is packed into a custom-made mold, and compacted under a strength of 102MPa;
[0047] (5) Curing: seal the formed module in a plastic airtight bag and place it in room temperature for curing. The curing time is 7 days.
[0048] Wherein, in step (3), the mass percentages of cement, lime, fly ash and activated carbon in the total amount of the obtained solidified rock debris soil mixture are shown in Table 1.
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Embodiment 9~ Embodiment 16
[0056] Embodiments 9-16 also solidified the drilling cuttings according to the steps of Embodiments 1-8. The difference is that after the optimal ratio of cement and lime added in Examples 1 to 8 is 5%, in the step (3) of Examples 9 to 16, cement, lime, fly ash and activated carbon each account for the resulting The mass percentage of the total amount of solidified rock debris-soil mixture is shown in Table 2.
[0057] Before solidification, the drilling cuttings were leached according to the GB5086.1-1997 method, and the COD value was detected according to the relevant detection method. The measured COD value of the drilling cuttings was 212mg / L.
[0058] After the above processing steps are completed, the cured solidified rock debris soil module is leached according to the GB5086.1-1997 method, and the COD concentration and pH are detected according to the relevant detection methods, and the solidification time is used to compare the various examples. The results are shown i...
Embodiment 17
[0063] This embodiment is used to illustrate a preferred specific implementation manner.
[0064] A method for solidifying natural gas drilling cuttings, comprising the steps of:
[0065] (1) Pretreatment: sieve drilling cuttings to obtain cuttings samples with a particle size not greater than 5mm;
[0066] (2) Regulate the water content: use water to adjust the water content of the cuttings sample to 40% ± 2%;
[0067] (3) solidification treatment: add cement, lime, fly ash and activated carbon to the rock chip sample of step (2) gained, mix and stir evenly, obtain solidified rock chip soil;
[0068] Among them, the mass dosage parts of cuttings samples, cement, lime, fly ash and activated carbon are respectively: 39.5 parts of cuttings samples, 5 parts of cement, 5 parts of lime, 50 parts of fly ash, and 0.5 parts of activated carbon;
[0069] (4) Compression molding: the solidified rock debris soil is packed into a custom-made mold, and compacted under a strength of 102MP...
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