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Fillet freshness detection method based on portable near-infrared spectrometer

A near-infrared spectrometer and detection method technology, applied in the field of measurement, can solve problems such as unfavorable detection, damage to samples, cumbersome operation, etc., and achieve the effect of easy operation

Pending Publication Date: 2020-08-11
HAINAN UNIVERSITY
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  • Claims
  • Application Information

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Problems solved by technology

Near-infrared spectrometer is the main tool for near-infrared spectrum analysis. Traditional laboratory near-infrared spectrometers have the disadvantages of large volume, cumbersome operation, and inconvenient portability. It is not conducive to detection anytime and anywhere, which limits the development of near-infrared spectroscopy technology.
In addition, in the application of variable selection methods, the newly developed variable selection algorithms are less used, especially the joint use of these algorithms, which makes the obtained results not ideal
[0003] Through the above analysis, the problems and defects of the prior art are: (1) the laboratory near-infrared spectrometer has a large volume, cumbersome operation, and is not easy to carry
[0004](2) The traditional fish fillet freshness detection method needs to destroy the sample during the operation, and the operation is cumbersome
[0005] The difficulties in solving the above problems and defects are as follows: (1) To measure the content of volatile base nitrogen (Total volatile base nitrogen, TVB-N) by traditional chemical method (Kjeldahl method), it is necessary to re-explore the experimental parameters

Method used

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  • Fillet freshness detection method based on portable near-infrared spectrometer
  • Fillet freshness detection method based on portable near-infrared spectrometer
  • Fillet freshness detection method based on portable near-infrared spectrometer

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Embodiment 1

[0068] The invention provides a method for detecting the freshness of fish fillets based on a portable near-infrared spectrometer. The method utilizes a portable near-infrared spectrometer for spectrum collection, Kjeldahl method for determining volatile base nitrogen, and related chemometric methods for data processing. . The whole process mainly includes the experimental part (sample preparation, spectrum acquisition and volatile basic nitrogen (TVB-N) determination) and the data processing part (outlier elimination, spectral preprocessing and optimal wavelength selection), specifically Proceed as follows:

[0069] 3.1 Experimental part

[0070] 1) Sample preparation: put the fish fillets into a plastic airtight bag and refrigerate at 4°C. At 0, 2, 4, 6, 8, and 10 days, 20 samples were taken for spectral collection and determination of volatile basic nitrogen.

[0071] 2) Spectrum acquisition: firstly perform software (BWSpec (v.4.11) software (B&W Tek, USA)) and near-inf...

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Abstract

The invention belongs to the technical field of measurement, and discloses a fillet freshness detection method based on a portable near-infrared spectrometer and the spectrometer. The portable near-infrared spectrometer is used for spectrum acquisition, total volatile basic nitrogen (TVB-N) is measured by virtue of a Kjeldahl determination method. A mathematical model between the spectral data andthe measured TVB-N content is built through a chemometrics method,variable selection is carried out by using a three-step combination strategy, a TVB-N value is predicted through the established model, and the freshness of the fillets is evaluated according to the TVB-N value. The defects of large volume, complicated operation, inconvenient carrying and the like of a laboratory near-infrared spectrometer are solved, the detection can be carried out anytime and anywhere, and the operation is simple and convenient. In addition, a three-step combination strategy is used for variable selection, and data show that the method can obtain a result superior to that of a single algorithm and two-step combination.

Description

technical field [0001] The invention belongs to the technical field of measurement, and in particular relates to a method for detecting the freshness of fish fillets based on a portable near-infrared spectrometer and a spectrometer. Background technique [0002] At present, as a fast and non-destructive analysis tool, near-infrared spectroscopy has been widely used in traditional Chinese medicine, petroleum, textiles, agricultural products and other fields. Near-infrared spectrometer is the main tool for near-infrared spectrum analysis. Traditional laboratory near-infrared spectrometers have the disadvantages of large volume, cumbersome operation, and inconvenient portability. It is not conducive to detection anytime and anywhere, which limits the development of near-infrared spectroscopy technology. In addition, in the application of variable selection methods, the newly developed variable selection algorithms are rarely used, especially the joint use of these algorithms, w...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/3563G01N21/359G01N31/00G01N31/16
CPCG01N21/3563G01N21/359G01N31/002G01N31/16G01N2021/3572
Inventor 云永欢余海东章程辉
Owner HAINAN UNIVERSITY
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