Oligopeptide, weight loss composition, preparation method and application
A composition and oligopeptide technology applied in the biological field to achieve the effect of inhibiting the activity of pancreatic lipase
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Embodiment 1
[0052] This embodiment provides a weight loss composition containing Ala-Pro-Tyr-Arg (APYR) oligopeptide, the preparation method of which is as follows:
[0053] Grind seabuckthorn seeds to 100 mesh and mix them with water at a mass ratio of 1:10 to obtain an aqueous solution of seabuckthorn seeds, adjust its pH to 6.5, and then add neutral protease (the mass ratio of neutral protease to crushed seabuckthorn seeds is 0.25:100 ), then stirred and hydrolyzed at 37°C for 2 hours, and then inactivated the enzyme at 95°C for 15 minutes after the hydrolysis to obtain the seabuckthorn seed protein hydrolyzate;
[0054]Centrifuge the above seabuckthorn seed protein hydrolyzate at 4°C and 8000 rpm for 20 minutes, and then take the supernatant and freeze-dry to obtain the weight loss composition containing APYR oligopeptide. As detected by HPLC, the content of APYR oligopeptide in the weight loss composition is 1.85g / 100g.
[0055] This embodiment also provides a method for purifying A...
Embodiment 2
[0063] This embodiment provides a weight loss composition containing Ala-Pro-Tyr-Arg (APYR) oligopeptide, the preparation method of which is as follows:
[0064] Pulverize the seabuckthorn seeds to 100 mesh and mix them with water at a mass ratio of 1:15 to obtain an aqueous solution of seabuckthorn seeds, adjust the pH to 5.0 and add trypsin (the mass ratio of pancreatin to crushed seabuckthorn seeds is 1.0:100), Then stir and hydrolyze at 25°C for 24 hours, and inactivate the enzyme at 85°C for 10 minutes after the hydrolysis to obtain the seabuckthorn seed protein hydrolyzate;
[0065] Centrifuge the above seabuckthorn seed protein hydrolyzate at 3°C and 10,000 rpm for 10 minutes, then take the supernatant and freeze-dry to obtain the weight loss composition containing APYR oligopeptide. As detected by HPLC, the content of APYR oligopeptide in the weight loss composition is 1.18g / 100g.
[0066] This embodiment also provides a method for purifying Ala-Pro-Tyr-Arg (APYR) o...
Embodiment 3
[0072] This embodiment provides a weight loss composition containing Ala-Pro-Tyr-Arg (APYR) oligopeptide, the preparation method of which is as follows:
[0073] After pulverizing seabuckthorn seeds to 100 meshes, mix them with water at a mass ratio of 1:12 to obtain an aqueous solution of seabuckthorn seeds, adjust its pH to 7.0, and then add pancreatin (the mass ratio of pancreatin to pulverized seabuckthorn seeds is 2.0:100 ), then stirred and hydrolyzed at 60°C for 15 hours, and inactivated the enzyme at 90°C for 20 minutes to obtain seabuckthorn seed protein hydrolyzate;
[0074] Centrifuge the above seabuckthorn seed protein hydrolyzate at 5°C and 6000 rpm for 15 minutes, then take the supernatant and freeze-dry to obtain the weight loss composition containing APYR oligopeptide. As detected by HPLC, the content of APYR oligopeptide in the weight loss composition is 1.02g / 100g.
[0075] This embodiment also provides a method for purifying Ala-Pro-Tyr-Arg (APYR) oligopept...
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