Fulvic acid sterilization deodorant as well as preparation method and application thereof
A technology of bactericidal deodorant and fulvic acid, applied in botanical equipment and methods, application, deodorization and other directions, can solve problems such as damage to physical and mental health, polluted air quality, hidden dangers to human health, etc., and achieve safety of raw materials and environmental compatibility. The effect of good capacitance and easy degradation
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Embodiment 1
[0031] Fulvic acid and dodecyltrimethylammonium chloride with a mass ratio of 42:1 were reacted in a water bath at 45°C for 3 hours, vacuum filtered and the filtrate was dried to obtain a fulvic acid surfactant. After washing the saponins, add an equal volume of deionized water to soak for 4 hours, squeeze the juice and filter through a 100-mesh sieve, and concentrate the filtrate to 1.3 g / cm3 to obtain saponins extract. Cinnamomum camphora was crushed through an 80-mesh sieve, and Cinnamomum camphora and petroleum ether were mixed at a material-to-liquid ratio of 1:20, and then ultrasonically extracted at 70°C for 50 minutes to obtain Cinnamomum camphora extract. Ginger was crushed through an 80-mesh sieve, and the ginger and absolute ethanol were mixed at a material-to-liquid ratio of 1:20, and then ultrasonically extracted at 70°C for 50 minutes to obtain a ginger extract. Crush mint through an 80-mesh sieve, mix mint and petroleum ether with a solid-liquid ratio of 1:12, s...
Embodiment 2
[0034] Fulvic acid and dodecyltrimethylammonium chloride with a mass ratio of 42:1 were reacted in a water bath at 50°C for 3.5 hours, vacuum filtered and the filtrate was dried to obtain a fulvic acid surfactant. After washing the saponins, add an equal volume of deionized water to soak for 4 hours, squeeze the juice and filter through a 100-mesh sieve, and concentrate the filtrate to 1.3 g / cm3 to obtain saponins extract. Cinnamomum camphora was crushed through an 80-mesh sieve, and Cinnamomum camphora and petroleum ether were mixed at a material-to-liquid ratio of 1:20, and then ultrasonically extracted at 70°C for 50 minutes to obtain Cinnamomum camphora extract. Ginger was crushed through an 80-mesh sieve, and the ginger and absolute ethanol were mixed at a material-to-liquid ratio of 1:20, and then ultrasonically extracted at 70°C for 50 minutes to obtain a ginger extract. Crush mint through an 80-mesh sieve, mix mint and petroleum ether with a solid-liquid ratio of 1:12,...
Embodiment 3
[0037]Fulvic acid and dodecyltrimethylammonium chloride with a mass ratio of 42:1 were reacted in a water bath at 60°C for 4 hours, vacuum filtered and the filtrate was dried to obtain a fulvic acid surfactant. After washing the saponins, add an equal volume of deionized water to soak for 4 hours, squeeze the juice and filter through a 100-mesh sieve, and concentrate the filtrate to 1.3 g / cm3 to obtain saponins extract. Cinnamomum camphora was crushed through an 80-mesh sieve, and Cinnamomum camphora and petroleum ether were mixed at a material-to-liquid ratio of 1:20, and then ultrasonically extracted at 70°C for 50 minutes to obtain Cinnamomum camphora extract. Ginger was crushed through an 80-mesh sieve, and the ginger and absolute ethanol were mixed at a material-to-liquid ratio of 1:20, and then ultrasonically extracted at 70°C for 50 minutes to obtain a ginger extract. Crush mint through an 80-mesh sieve, mix mint and petroleum ether with a solid-liquid ratio of 1:12, so...
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