Polyvinyl chloride composition, polyvinyl chloride powder and production method thereof
A technology of polyvinyl chloride powder and a production method, applied in the field of polyvinyl chloride powder, can solve the problems of reducing product odor quality, poor thermal stability of polyvinyl chloride powder, pungent odor of stabilizers, etc., and achieve the effect of reducing odor.
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Embodiment 1
[0040] First, mix 8.6 kilograms of vinyl chloride monomers, 8.6 grams of dispersant compound (comprising 800ppm model dispersant of BC20 (manufactured by Changchun Chemical Industry), 100ppm model of dispersant agent BL02 (manufactured by Changchun Chemical Industry), and 100ppm of hydroxypropyl base methyl cellulose) and 16 kg of water to form a mixed solution. Then, 8.6 grams of initiator compound (comprising 150ppm of diisobutyryl peroxide and 850ppm of 1,1,3,3-tetramethylbutyl peroxyneodecanoate) was added to the mixed solution, and the temperature The temperature was raised to 51°C for suspension polymerization. When the pressure drop reaches 1.5 kg, the unreacted vinyl chloride monomer in the formed polyvinyl chloride slurry is removed, and ammonia water is added to the polyvinyl chloride slurry to adjust the pH value to 7.0. Next, remove the water from the polyvinyl chloride slurry and dry it with a small fluidized bed dryer. After drying at 70°C for 2 hours, the poly...
Embodiment 2
[0043] Embodiment 2 to embodiment 5 are to use the same preparation method as the preparation method of the polyvinyl chloride powder of embodiment 1, the difference is that embodiment 2 and embodiment 3 use different initiators respectively, and its formula and reaction The conditions are respectively shown in Table 1, and will not be repeated here.
[0044] In the polyvinyl chloride powder of Example 2, the odor intensity of the olfactory judge is 3.6, the reading value of the odor intensity measured by the electronic nose is 89, and the yellowness value is 5.2%. In the polyvinyl chloride powder of Example 3, the odor intensity of the olfactory judge is 3.6, the reading value of the odor intensity measured by the electronic nose is 85, and the yellowness value is 5.6%. In the polyvinyl chloride powder of Example 4, the odor intensity of the olfactory judge is 3.5, the odor intensity reading value measured by the electronic nose is 56, and the yellowness value is 4.0%. In th...
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