Electrolyte and battery
An electrolyte and additive technology, applied in the field of lithium-ion batteries, can solve the problems of deteriorating the electrochemical performance of lithium batteries, increasing the acidity value and chromaticity value of the electrolyte, and failing to achieve the effect of DTD, etc.
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[0026] The preparation method of the present invention will be further described in detail in conjunction with specific examples below. It should be understood that the following examples are only for illustrating and explaining the present invention, and should not be construed as limiting the protection scope of the present invention. All technologies realized based on the above contents of the present invention are covered within the scope of protection intended by the present invention.
[0027] The experimental methods used in the following examples are conventional methods unless otherwise specified; the reagents and materials used in the following examples can be obtained from commercial sources unless otherwise specified.
[0028] Both reactant (II) and reactant (III) in the examples of the present invention were purchased from Shengtai Chemical Co., Ltd.
Embodiment 1
[0030] Embodiment 1 proposes an electrolyte solution and a battery.
[0031] (1) Additives and their preparation methods
[0032] Using formula 1, the reactant (II) and the reactant (III) are mixed according to the mass ratio of about 1:1 at a temperature of 45°C and a pH of 9.0 for about 50 minutes to obtain the additive (I), such as Formula (1) shown. And carry out mass spectrometry analysis to additive (Ι), as figure 1 As shown, its main peak is at 91, showing the structural characteristics of SO2-CN, and simultaneously, its peak at 203 corresponds to the molecular characteristics of additive (I).
[0033]
[0034] (2) Electrolyte
[0035] A mixed solvent of ethylene carbonate and diethyl carbonate with a mass ratio of 3:7 was used, and LiPF was added 6 And stir fully to obtain the reference electrolyte. Among them, electrolyte-based mass meter, LiPF 6 The mass fraction is 12%. Then add the additive (I) with a mass fraction of 0.01% and vinyl sulfate (DTD) with a ...
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