Low-resilience alkali-free liquid accelerator and preparation method thereof
A low-rebound, accelerator technology, applied in the field of building concrete admixtures, can solve the problems of low compressive strength in the early stage, containing toxic substances, and complicated preparation process of alkali-free accelerators, so as to improve the compressive strength and Stability, simple preparation method, and the effect of being beneficial to large-scale industrial production and application
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Embodiment 1
[0028] In this embodiment, in terms of mass percentage, the raw materials of the low-resilience alkali-free liquid accelerator are composed of: 55% aluminum sulfate octadecahydrate, 6% aluminum dihydrogen phosphate, 12% diethanolamine, 1% triethanolamine, 1% sodium citrate, 0.5% composite enhancer, 2% phosphoric acid and 22.5% water.
[0029] In this example, the specific synthesis steps of the quick-setting agent are as follows: add water, sodium citrate and composite reinforcing agent to the reaction pot in sequence, start stirring, adjust the speed to 300r / min, start heating, set the temperature at 50°C, When the solution in the reaction pot is colorless and transparent, add aluminum sulfate octadecahydrate and aluminum dihydrogen phosphate to the reaction pot in turn, and continue to stir at this temperature for 1 hour, then slowly add diethanolamine and triethanolamine to the In the reaction pot, and continue to stir at this temperature for 1.5h, finally add phosphoric ac...
Embodiment 2
[0031] In this embodiment, in terms of mass percentage, the raw materials of the low-rebound alkali-free liquid accelerator are composed of: 53% aluminum sulfate octadecahydrate, 6% aluminum dihydrogen phosphate, 10% diethanolamine, 1% triethanolamine, 2% vitamin C, 0.6% complex enhancer, 2% phosphoric acid and 25.4% water.
[0032] In this example, the specific synthesis steps of the quick-setting agent are as follows: add water, vitamin C and composite enhancer to the reaction pot in sequence, start stirring, adjust the speed to 200r / min, start heating, set the temperature at 50°C, and wait for When the solution in the reaction pot is colorless and transparent, add aluminum sulfate octadecahydrate and aluminum dihydrogen phosphate to the reaction pot in turn, and continue stirring at this temperature for 1 hour, then slowly add diethanolamine and triethanolamine to the reaction pot pot, and continue to stir at this temperature for 1.5 hours, and finally add phosphoric acid t...
Embodiment 3
[0034] In this embodiment, in terms of mass percentage, the raw materials of the low-resilience alkali-free liquid accelerator are as follows: 55% aluminum sulfate octadecahydrate, 4% aluminum dihydrogen phosphate, 1% ethanolamine, 10% diethanolamine, 0.5 % triethanolamine, 1% vitamin C, 0.8% complex enhancer, 3% phosphoric acid and 24.7% water.
[0035] In this example, the specific synthesis steps of the quick-setting agent are as follows: add water, vitamin C and composite enhancer to the reaction pot in sequence, start stirring, adjust the speed to 200r / min, start heating, set the temperature at 50°C, and wait for When the solution in the reaction pot is colorless and transparent, add aluminum sulfate octadecahydrate and aluminum dihydrogen phosphate to the reaction pot in turn, and continue stirring at this temperature for 1 hour, then slowly add ethanolamine, diethanolamine and triethanolamine into the reaction pot, and continue to stir at this temperature for 1.5 hours,...
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Abstract
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