Method for producing volatile chemical and fermentation device
A manufacturing method and technology of chemicals, applied in the directions of biochemical cleaning devices, biochemical equipment and methods, enzymology/microbiology devices, etc., can solve problems such as pressure rise, danger, reduction of chemical recovery, etc., to reduce losses Effect
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[0104] Hereinafter, the present invention will be described in detail with reference to Examples and Comparative Examples. In all the examples and comparative examples, experiments were performed with the ventilation piping, the ventilation port, and the reflux condenser of the culture apparatus always open.
reference example 1
[0105] (Reference example 1) Determination of ethanol
[0106] The ethanol concentration was measured by comparison with a standard product under the gas chromatography conditions shown below.
[0107] Equipment: SHIMADZU GAS CHROMATOGRAPH GC-2010 (SHIMADZU)
[0108] Column: TC-BOND Q 0.25mm*30mm
[0109] Mobile Phase: Helium
[0110] Detection method: FID
[0111] Velocity: 40cm / s
[0112] Temperature: 250°C.
reference example 2
[0113] (Reference example 2) Determination of sugar
[0114] The sugar concentration was quantified by comparison with a standard under the HPLC conditions shown below.
[0115] Equipment: SHIMADZU HPLC system (Shimadzu)
[0116] Column: HILICpak VG-50 4E (Shodex)
[0117] Mobile phase: acetonitrile: water = 3:1
[0118] Detection method: RI detector
[0119] Flow rate mobile phase: 0.6mL / min
[0120] Temperature: 40°C.
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