Thermosetting electrolyte composition for lithium secondary battery, gel polymer electrolyte prepared therefrom, and lithium secondary battery comprising same
A lithium secondary battery and gel polymer technology, which is applied in the direction of electrolyte immobilization/gelation, electrolyte battery manufacturing, non-aqueous electrolyte battery, etc., can solve the problem of increased interface resistance, low stability, and reduced battery wettability and other problems to achieve the effect of preventing pre-gelation
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Embodiment 1
[0168] (Preparation of Thermosetting Electrolyte Composition)
[0169] LiPF 6 and LiFSi(LiN(SO 2 f) 2 ) was dissolved in 94g of non-aqueous organic solvent in which ethylene carbonate (EC) and dimethyl carbonate (DMC) were mixed in a volume ratio of 15:85, so that LiPF 6 and LiFSi each at a concentration of 1.0 M, after which by adding 5.0 g of a polymer comprising units represented by formula 1 (R is –CH 2 -CH 2 -, k: 84mol, m: 14mol, n: 2mol, weight average molecular weight (Mw): 61,000) and 1.0g vinylene carbonate (VC) to prepare a thermosetting electrolyte composition.
[0170] (Preparation of Electrode Assembly)
[0171] The positive electrode active material (Li(Ni 0.8 mn 0.1 co 0.1 )O 2 ), a conductive agent (carbon black) and a binder (polyvinylidene fluoride: PVDF) were added to N-methyl-2-pyrrolidone (NMP) as a solvent in a weight ratio of 94:3:3 to prepare Positive electrode active material slurry (solid content: 48% by weight). A 100 μm thick positive el...
Embodiment 2
[0177] A lithium secondary battery comprising a gel polymer electrolyte was prepared in the same manner as in Example 1, except that LiPF 6 and LiFSi(LiN(SO 2 f) 2 ) is dissolved in 94g of non-aqueous organic solvent, making LiPF 6 and LiFSi each at a concentration of 1.0 M, after which by adding 5.0 g of a polymer comprising units represented by formula 1 (R is –CH 2 -CH 2 -, k: 73mol, m: 21mol, n: 6mol, weight average molecular weight (Mw): 65,000) and 1.0g vinylene carbonate (VC) to prepare a thermosetting electrolyte composition.
Embodiment 3
[0179] A lithium secondary battery comprising a gel polymer electrolyte was prepared in the same manner as in Example 1, except that LiPF 6 and LiFSi(LiN(SO 2 f) 2 ) is dissolved in 94g of non-aqueous organic solvent, making LiPF 6 and LiFSi each at a concentration of 1.0 M, after which by adding 5.0 g of a polymer comprising units represented by formula 1 (R is –CH 2 -CH 2 -, k: 86mol, m: 8mol, n: 6mol, weight average molecular weight (Mw): 62,000) and 1.0g vinylene carbonate (VC) to prepare a thermosetting electrolyte composition.
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