Unlock instant, AI-driven research and patent intelligence for your innovation.

A kind of preparation method of quasi-single crystal pure copper

A pure copper, single crystal technology, applied in the direction of manufacturing tools, furnace types, metal rolling, etc., can solve the problem of high energy consumption, and achieve the effect of low cost and high efficiency

Active Publication Date: 2021-12-17
CHINALCO MATERIALS APPL RES INST CO LTD
View PDF12 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the hot-type continuous casting method is mainly used in the industry to prepare single crystal copper. Since the hot-type continuous casting has high requirements for equipment and needs to be carried out at high temperature for a long time, the energy consumption is high.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A kind of preparation method of quasi-single crystal pure copper

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] (1) Selecting a pure copper rod with an equiaxed grain structure as a blank;

[0019] (2) Carry out drawing treatment to pure copper bar, the total deformation of drawing is 75%, and the diameter reduction of each pass is 0.5mm;

[0020] (3) Inductively heat the head area of ​​the pure copper rod obtained by the drawing process under a protective atmosphere, with a first uniform heating area and a first low-temperature radiation area, the temperature of the first uniform heating area is 600 ° C, and the heat preservation The time is 40h, the heating rate is 2°C / min, the length of the first uniform heating zone is 20mm, and the temperature of the first low-temperature radiation zone is controlled at 280°C, thereby forming a seed crystal at the head;

[0021] (4) The pure copper bar whose head is formed with a seed crystal is sequentially placed in the second uniform heating zone and the second low-temperature radiation zone, and the on-line continuous induction heating a...

Embodiment 2

[0023] (1) Selecting a pure copper rod with an equiaxed grain structure as a blank;

[0024] (2) Drawing treatment is carried out to pure copper bar, the total deformation of drawing is 60%, and the diameter reduction of each pass is 1mm;

[0025] (3) Inductively heat the head area of ​​the pure copper rod obtained by the drawing process under a protective atmosphere, with a first uniform heating area and a first low-temperature radiation area, the temperature of the first uniform heating area is 500 ° C, and the heat preservation The time is 50h, the heating rate is 1°C / min, the length of the first uniform heating area is 5mm, and the temperature of the first low-temperature radiation area is controlled at 260°C, so as to form a seed crystal at the head;

[0026] (4) The pure copper rod with the head forming the seed crystal is sequentially placed in the second uniform heating zone and the second low-temperature radiation zone, and the on-line continuous induction heating ann...

Embodiment 3

[0028] (1) Selecting a pure copper rod with an equiaxed grain structure as a blank;

[0029] (2) Drawing treatment is carried out to pure copper rod, the total deformation of drawing is 90%, and the diameter reduction of each pass is 1mm;

[0030] (3) Inductively heat the head area of ​​the pure copper rod obtained by the drawing process under a protective atmosphere, with a first uniform heating area and a first low-temperature radiation area, the temperature of the first uniform heating area is 700 ° C, and the heat preservation The time is 6 hours, the heating rate is 5°C / min, the length of the first uniform heating zone is 10mm, and the temperature of the first low-temperature radiation zone is controlled at 290°C, so as to form a seed crystal at the head;

[0031] (4) In the second uniform heating zone and the second low-temperature radiation zone, the pure copper rod with the head forming the seed crystal is subjected to online continuous induction heating and annealing ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
lengthaaaaaaaaaa
lengthaaaaaaaaaa
thicknessaaaaaaaaaa
Login to View More

Abstract

The invention discloses a method for preparing a kind of single crystal pure copper. The initial pure copper bar or strip / foil is deformed by drawing or cold rolling, and the end of the deformed pure copper is subjected to induction heating to achieve seed crystal growth, and finally the Continuous annealing can realize the directional growth of seed crystals along the length direction, thereby forming very coarse crystal grains. This method adopts low temperature and low cost, and is suitable for industrial production.

Description

technical field [0001] The invention relates to the technical field of preparation of high-performance copper materials for communication, in particular to a preparation method of quasi-single crystal pure copper. Background technique [0002] Pure copper has excellent electrical conductivity and signal fidelity performance, and its impurities and structure have a great influence on conductivity and fidelity performance. With the development of purification technology and the emergence of high-purity copper, the electrical conductivity of pure copper has been significantly improved. However, it is difficult to improve its conductivity and fidelity performance by further improving its purity. The grain boundaries in copper will reduce the conductivity and signal fidelity. Single crystal copper has a wide range of application values ​​in the field of electronic communication due to its superior comprehensive properties. At present, the hot-type continuous casting method is ma...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/02C22F1/08C21D9/00C21D9/46C21D9/52B21B3/00
CPCC22F1/02C22F1/08C21D9/0075C21D9/46C21D9/52B21B3/00B21B2003/005
Inventor 王金华娄花芬张曦陈忠平向朝建杨春秀莫永达
Owner CHINALCO MATERIALS APPL RES INST CO LTD