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Preparation method of orange peel pectin-based porous water-absorbing edible gel

A technology of edible gel and water absorption by pores, which is applied in the field of polymer material preparation, can solve the problems of uncommon natural degradable raw materials and cross-linking agent gels, and gels that are difficult to eat, and achieves a pollution-free preparation process. , The method is simple and easy to operate, and the effect is environmentally friendly.

Inactive Publication Date: 2021-02-02
QILU UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these gels have not broken through the structure of traditional water-absorbing resins, and it is difficult to serve as edible gels.
However, there are currently reports on gels with edible properties, pure natural degradable raw materials and cross-linking agent gels.

Method used

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  • Preparation method of orange peel pectin-based porous water-absorbing edible gel

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] At room temperature, add 1 part of fructose to 66 parts of deionized water, under stirring at 300 rpm, add 1 part of citric acid, 0.25 part of chitosan and 0.5 part of urea, after the dispersion is uniform, continue to stir at 300 rpm The reaction was stirred for 15 minutes at a constant stirring speed. Pour the obtained product into a hydrothermal kettle and heat it in an oven at 100° C. for 3.5 hours, then take out the sample, wash it with deionized water, and freeze-dry it in a vacuum dryer to obtain the product. It is measured that at room temperature, the multiple of deionized water absorbed reaches 3400% of the gel mass after drying, and the appearance is as attached figure 1 shown.

Embodiment 2

[0022] At room temperature, add 1 part of fructose to 16.5 parts of deionized water, and under stirring at 200 rpm, add 0.25 part of citric acid, 1 part of chitosan and 0.25 part of urea. The reaction was stirred for 15 minutes at a constant stirring speed. Pour the obtained product into a hydrothermal kettle and heat it in an oven at 105° C. for 2.5 hours, then take out the sample, wash it with deionized water, and freeze-dry it in a vacuum dryer to obtain the product. It is measured that at room temperature, the deionized water absorption multiple reaches 3200% of the gel mass after drying.

Embodiment 3

[0024] At room temperature, add 1 part of fructose to 33 parts of deionized water, and under stirring at 100 rpm, add 1.5 parts of citric acid, 1.5 parts of chitosan and 0.5 part of urea. The reaction was stirred for 30 minutes at a constant stirring speed. Pour the obtained product into a hydrothermal kettle and heat it in an oven at 105° C. for 3 hours, then take out the sample, wash it with deionized water, and freeze-dry it in a vacuum dryer to obtain the product. It is measured that at room temperature, the deionized water absorption multiple reaches 2800% of the gel mass after drying.

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Abstract

The invention discloses a preparation method of orange peel pectin-based porous water-absorbing edible gel, which comprises the steps of dissolving fructose in deionized water, completely dissolving,sequentially adding chitosan, citric acid and urea, carrying out crosslinking reaction, pouring the obtained product into a hydrothermal kettle, carrying out sufficient hydrothermal reaction in an oven, taking out the sample, cooling, cleaning with deionized water, and freeze-drying to obtain the product. According to the invention, a bio-based natural degradable material, namely, fructose is usedas a matrix, chitosan, citric acid and urea are added, and a cross-linking reaction is carried out, so that the non-toxic, porous and edible water-absorbing gel is prepared, and the water-absorbing gel not only is degradable, but also is edible and convenient to carry.

Description

technical field [0001] The invention belongs to the technical field of polymer material preparation, and in particular relates to a preparation method of orange peel pectin-based porous water-absorbing edible gel. Background technique [0002] Gel is a kind of hydrophilic polymer with a cross-linked network structure, which can absorb a large amount of water and retain water but is insoluble in water. Macromolecule or macromolecular aggregates, they can quickly swell and balance in water and can maintain their shape and three-dimensionality Spatial network structure. On the one hand, hydrogels are solid macroscopically and have a certain shape; on the other hand, hydrogels have solution properties at the molecular level, allowing water-soluble molecules to diffuse into them. The particularity of hydrogel structure makes it widely used in health, agriculture, gardening and other fields. In recent years, some new uses of hydrogel have emerged, such as controlled delivery and...

Claims

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Application Information

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IPC IPC(8): C08J9/28C08J3/075C08J3/24C08L5/08C08K5/092C08K5/21C08K5/1545
CPCC08J9/28C08J3/075C08J3/24C08J2305/08C08K5/092C08K5/21C08K5/1545
Inventor 宋兆萍赵书乾李伟高腾达郑德庆刘建业邱晶
Owner QILU UNIV OF TECH