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Process and system for producing refined salt by using salt production waste liquid

A technology for refining salt and waste liquid, which is applied in the field of salt production and can solve problems such as salt agglomeration and clogging

Active Publication Date: 2021-05-18
肥城胜利盐业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Aiming at the problems that the existing process of producing refined salt by using salt-making waste liquid is easy to block and the obtained salt is easy to agglomerate, the present invention provides a process and system for producing refined salt by using salt-making waste liquid. Blockage and agglomeration of refined salt occur during the process, thereby ensuring continuous and stable salt production and improving production efficiency

Method used

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  • Process and system for producing refined salt by using salt production waste liquid
  • Process and system for producing refined salt by using salt production waste liquid
  • Process and system for producing refined salt by using salt production waste liquid

Examples

Experimental program
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Effect test

Embodiment 1

[0027] The salt-making waste liquid was collected from the first salt-making area of ​​the company's salt factory, and the sampling and analysis results are shown in Table 1:

[0028] Table 1 The chemical composition of the salt-making waste liquid collected in the first salt-making district of our company

[0029]

[0030] A process for producing refined salt from salt-making waste liquid, comprising the steps of:

[0031] (1) Filtration and preheating: Use a semi-permeable membrane to filter the salt-making waste liquid, increase the concentration of the salt-making waste liquid to not less than 28°Be', and then enter the preheater for preheating. The preheating temperature is 80°C. The heat time is 15min, and the primary waste liquid is obtained;

[0032] (2) Evaporation and thickening: the primary waste liquid is heated to 110°C for 60 minutes for evaporation to generate a secondary waste liquid with a concentration of 35°Be';

[0033] (3) Cooling and crystallization:...

Embodiment 2

[0040] The salt-making waste liquid was collected from the fourth salt-making area of ​​the company's salt factory, and the sampling and analysis results are shown in Table 3:

[0041] Table 3 The chemical composition of the salt-making waste liquid collected in the fourth salt-making district of our company

[0042]

[0043] A process for producing refined salt from salt-making waste liquid, comprising the steps of:

[0044] (1) Filtration and preheating: Use semi-permeable membrane to filter the salt-making waste liquid, increase the concentration of the salt-making waste liquid to not less than 28°Be', and then enter the preheater for preheating. The preheating temperature is 70°C. The heating time is 30min, and the primary waste liquid is obtained;

[0045] (2) Evaporation and thickening: the primary waste liquid is heated to 113°C for 45 minutes of evaporation time to generate a secondary waste liquid with a concentration of 32°Be';

[0046] (3) Cooling and crystalli...

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Abstract

The invention relates to the technical field of salt production, in particular to a process for producing refined salt by using salt production waste liquid. The process comprises the following steps of: (1) filtering and preheating: filtering the salt production waste liquid by using a semipermeable membrane, and preheating the waste liquid in a preheater to obtain primary waste liquid; (2) evaporation and thickening: heating and evaporating the primary waste liquid to generate secondary waste liquid with the concentration of 32-35 degrees Be'; (3) cooling and devitrifying: cooling the secondary waste liquid, and filtering to remove the secondary waste liquid to obtain crystallized salt slurry; (4) washing and devitrification: enabling crystallized salt slurry to enter a salt leaching device for saturated brine washing, enabling the washed crystallized salt slurry to enter a salt storage bin and then enter a centrifugal machine through a cyclone to dewater the washed crystallized salt slurry so as to obtain wet salt, and enabling brine mother liquor removed by the centrifugal machine to flow back to the salt leaching device; and (5) drying. By optimizing the process, the phenomena of blockage and refined salt caking in the salt manufacturing process are avoided, and the continuity and stability of salt manufacturing production are ensured.

Description

technical field [0001] The invention relates to the technical field of salt production, in particular to a process and a system for producing refined salt by utilizing salt production waste liquid. Background technique [0002] Salt is the mother of the chemical industry and has a wide variety of uses. In the salt production process, a large amount of salt-making waste liquid will be produced, with a concentration of about 27°Be', containing a large amount of salt, and direct discharge will cause environmental pollution. Therefore, it is necessary to comprehensively utilize the salt-making waste liquid to improve resources. utilization rate. Based on this, patent ZL200710057195.3 discloses a preparation process for producing refined salt using salt-making waste liquid as raw material. The advanced vacuum salt making technology and salt washing process can produce high-quality industrial salt and improve the output and quality of industrial salt; however, this process is la...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01D3/06
CPCC01D3/06
Inventor 张刚贾启庞学雷王立宽纪培良
Owner 肥城胜利盐业有限公司
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