Method for establishing UPLC fingerprint spectrum of anti-hysteritis soft capsule
A technique for fingerprinting and establishing methods, which is applied in the field of Kanggongyan soft capsules, can solve the problems that the fingerprints and detection methods of Kanggongyan soft capsules have not been reported, and achieve good stability, high precision and good repeatability Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment Construction
[0064] The present invention will be further described below in conjunction with the examples, but not as a basis for limiting the present invention.
[0065] Example. A method for establishing the UPLC fingerprint of anti-gongyan soft capsules, the establishment steps are:
[0066] (1) Preparation of mixed reference solution: Accurately weigh appropriate amounts of norisoboldine, leonurine hydrochloride, forsythoside B, verbascoside, chrysoside, and isorrascoside, put them in a volumetric flask, add 50% Diluted with methanol and shaken well, the obtained concentrations were 0.05 (norisoboldine), 0.15 (leonurine hydrochloride), 0.15 (forsythoside B), 0.15 (verbasoside), 0.15 (chryposide), 0.15(isoverbasin) mg·mL -1 mixed reference solution.
[0067] (2) Preparation of test solution: take 1.0g of anti-gongyan soft capsule content, accurately weigh it, place it in a round-bottomed flask, accurately add 50 mL of 50% methanol, weigh it, reflux for 1 hour, let it cool, and weigh...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com