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Composition for preparing vigor-preserving soup, vigor-preserving soup product and fingerprint spectrum determination and quality detection method of vigor-preserving soup product

A fingerprint and determination method technology, which is applied to medical preparations containing active ingredients, measuring devices, drug combinations, etc., can solve the problem of not detecting the fingerprint of Baoyuan Decoction, etc.

Active Publication Date: 2021-07-02
XIAMEN TRADITIONAL CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] At present, there is no method for detecting the fingerprints of Baoyuan Tang and its products, the method of establishing standard fingerprints and the research on using it for quality control

Method used

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  • Composition for preparing vigor-preserving soup, vigor-preserving soup product and fingerprint spectrum determination and quality detection method of vigor-preserving soup product
  • Composition for preparing vigor-preserving soup, vigor-preserving soup product and fingerprint spectrum determination and quality detection method of vigor-preserving soup product
  • Composition for preparing vigor-preserving soup, vigor-preserving soup product and fingerprint spectrum determination and quality detection method of vigor-preserving soup product

Examples

Experimental program
Comparison scheme
Effect test

preparation Embodiment 1

[0052] Preparation Example 1: Preparation of Baoyuan Decoction

[0053] See Table 1 below for the raw material formula of Baoyuan soup.

[0054] [Table 1]

[0055]

[0056]

[0057] Preparation process: put the raw materials listed in Table 1 in a 3L decoction pot, add three slices of ginger (~9.00g), decoct twice, add 1800ml of water for the first decoction, soak for 30 minutes, heat to boil (about 13 minutes), decoct Boil for 45 minutes, filter while hot (200 mesh) to get the first decoction liquid, add 1350ml of water to the second decoction, heat to boil (about 9 minutes), decoct for 35 minutes, filter while hot (200 mesh), get the second decoction liquid, Combine the two liquid medicines, concentrate under reduced pressure (temperature 60°C) to 300ml, and obtain Baoyuan Decoction.

preparation Embodiment 2

[0058] Preparation Example 2: Preparation of Baoyuan Decoction Extract Powder

[0059] The Baoyuantang obtained in Preparation Example 1 was pre-frozen and then freeze-dried (temperature -40°C, pressure 20Pa) for 24 hours to obtain Baoyuantang freeze-dried powder, which was sealed in a ziplock bag and stored in a drying cabinet.

[0060] Properties: brown to brown powder; sweet, slightly bitter.

preparation Embodiment 3

[0061] Preparation Example 3: According to a method similar to Preparation Example 2, 17 batches of Baoyuantang extract powder were prepared.

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Abstract

The invention provides a vigor-preserving soup, a product thereof, a fingerprint spectrum determination method and a quality detection method thereof. The fingerprint spectrum determination method comprises the following steps: 1) preparing a test sample solution; 2) preparing a mixed reference substance solution; 3) setting chromatographic conditions, wherein a mobile phase is acetonitrile (A)-water (B), gradient elution is performed for 0-20 min with16%-17% A, for 20-35 min with 17%-19.5% A, for 35-55 min with 19.5%-26% A, for 55-75 min with 26%-29% A, and for 75-110 min with 29%-42% A; the flow velocity is 1.0 ml / min; the column temperature is 35 DEG C; the chromatographic column is Thermo BDS HYPERSIL C18 250 * 4.6 mm, 5 [mu] m; the detection wavelength is 203 nm; 4) carrying ou tdetermination; and 5) performing data matching on the liquid chromatograms of the test sample solution and the mixed reference substance solution to obtain the standard fingerprint spectrum.

Description

technical field [0001] The invention belongs to the field of traditional Chinese medicine, and more specifically relates to an HPLC fingerprint determination method of Baoyuan decoction extract. Background technique [0002] Baoyuan soup is a classic recipe. "Concise Medicine" (Ming·Sun Zhihong) records that "treat weak vitality, mental fatigue, slow muscles, poor diet, and blue face. white, sleeping and sleeping peacefully,...and miscellaneous syndromes, all belong to weakness and should be taken.” The prescription is: 1 qian of ginseng, 2 qian of astragalus, 5 fen of licorice, and 2 fen of cinnamon. The preparation method and usage are: add a slice of ginger to the right , Shuijianbi.Dosage form: decoction. [0003] There are no substance benchmark studies for this party. [0004] Traditional Chinese medicine fingerprint technology is more and more used in the quality control of traditional Chinese medicine because it can comprehensively mark the characteristics of the...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/86A61K36/9068A61P1/14
CPCG01N30/8686A61K36/258A61K36/481A61K36/484A61K36/54A61K36/9068A61P1/14A61K2236/331A61K2236/39A61K2236/51A61K2300/00Y02A50/30
Inventor 关斌许舒瑜阳丽华肖惠琳许玉珍陈晓琳南淑华曾智发郑珊珊
Owner XIAMEN TRADITIONAL CHINESE MEDICINE