A kind of electric heating aromatherapy liquid and preparation method thereof
A technology of electric heating incense and extract, applied in botany equipment and methods, chemicals for biological control, pest repellent, etc., can solve the problems of human harm, poor persistence of mosquito repellent, inconvenient use, etc., and achieve Avoid irritation, good repellent effect
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Embodiment 1
[0025] (1) Preparation of lavender essential oil: wash and pulverize lavender, pass through a 40-mesh sieve, use n-hexane as the extraction solvent, and use n-hexane that is 4 times the volume of lavender, soak the pulverized lavender in n-hexane for 15 minutes, At the same time, microwave radiation is used so that the microwave power is 650W, and then ultrasonic extraction is performed. Using 25KHz ultrasonic waves, ultrasonic extraction is performed for 20 minutes, and the obtained extract is distilled under reduced pressure to obtain an ultrasonic extract. The ultrasonic extraction residue is added to 4 times the weight of water, and input into the autoclave so that the pressure in the autoclave is 6MPa, high-pressure decoction 15min, filter to obtain the high-pressure decoction and high-pressure extraction residue, then carry out vacuum distillation to the high-pressure decoction to obtain the high-pressure extract, and the high-pressure extract Mix with ultrasonic extract ...
Embodiment 2
[0029] (1) Preparation of lavender essential oil: Wash and pulverize lavender, pass through a 50-mesh sieve, use n-hexane as the extraction solvent, and use n-hexane that is 5 times the volume of lavender, soak the pulverized lavender in n-hexane for 18 minutes, and soak it in the soaked At the same time, microwave radiation is used so that the microwave power is 700W, and then ultrasonic extraction is performed, using 28KHz ultrasonic waves, ultrasonic extraction for 22min, the resulting extract is distilled under reduced pressure to obtain an ultrasonic extract, and the ultrasonic extraction residue is added to 5 times the weight of water, input into the autoclave so that the pressure in the autoclave is 7MPa, high-pressure decoction 18min, filtration to obtain the high-pressure decoction and high-pressure extraction residue, then the high-pressure decoction is subjected to reduced-pressure distillation to obtain the high-pressure extract, and the high-pressure extract Mix wi...
Embodiment 3
[0033] (1) Preparation of lavender essential oil: Wash and pulverize lavender, pass through a 60-mesh sieve, use n-hexane as the extraction solvent, and use n-hexane that is 6 times the volume of lavender, soak the pulverized lavender in n-hexane for 20 minutes, and soak in the soaked At the same time, microwave radiation is used so that the microwave power is 750W, and then ultrasonic extraction is performed. Using 40KHz ultrasonic waves, ultrasonic extraction is performed for 25 minutes, and the obtained extract is distilled under reduced pressure to obtain an ultrasonic extract. Add 6 times the weight of water to the ultrasonic extraction residue, and input into the autoclave so that the pressure in the autoclave is 8MPa, high-pressure decoction 20min, filter to obtain the high-pressure decoction and high-pressure extraction residue, then carry out vacuum distillation to the high-pressure decoction to obtain the high-pressure extract, and the high-pressure extract Mix with u...
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